methyl (Z)-2-(isothioureidomethyl)-3-(4-methoxyphenyl)-2-propenoate hydrobromide

Base Information

Chemical Name:methyl (Z)-2-(isothioureidomethyl)-3-(4-methoxyphenyl)-2-propenoate hydrobromide
CAS No.:1255193-92-0
Molecular Formula:BrH*C₁₃H₁₆N₂O₃S
Molecular Weight:361.26
Hs Code.:

Synonyms:methyl (Z)-2-(isothioureidomethyl)-3-(4-methoxyphenyl)-2-propenoate hydrobromide

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Chemical Property of methyl (Z)-2-(isothioureidomethyl)-3-(4-methoxyphenyl)-2-propenoate hydrobromide

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Technology Process of methyl (Z)-2-(isothioureidomethyl)-3-(4-methoxyphenyl)-2-propenoate hydrobromide

There total 3 articles about methyl (Z)-2-(isothioureidomethyl)-3-(4-methoxyphenyl)-2-propenoate hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 17356-08-0
thiourea

: 213999-88-3
methyl (2Z)-2-(bromomethyl)-3-(4-methoxyphenyl)prop-2-enoate

: 1255193-92-0
methyl (Z)-2-(isothioureidomethyl)-3-(4-methoxyphenyl)-2-propenoate hydrobromide

Guidance literature:: In water; acetone; at 25 ℃; for 1h;
DOI:10.3998/ark.5550190.0011.b24

Reference yield:

: 115240-92-1
methyl 2-[hydroxy(4-methoxyphenyl)methyl]prop-2-enoate

: 1255193-92-0
methyl (Z)-2-(isothioureidomethyl)-3-(4-methoxyphenyl)-2-propenoate hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: lithium bromide / acetonitrile / 20 °C / Acidic conditions

2: acetone; water / 20 °C

With lithium bromide; In water; acetone; acetonitrile;
DOI:10.1016/j.ejmech.2013.10.017

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1255193-92-0
methyl (Z)-2-(isothioureidomethyl)-3-(4-methoxyphenyl)-2-propenoate hydrobromide

Guidance literature:: Multi-step reaction with 3 steps

1: 1,4-diaza-bicyclo[2.2.2]octane

2: lithium bromide / acetonitrile / 20 °C / Acidic conditions

3: acetone; water / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; lithium bromide; In water; acetone; acetonitrile;
DOI:10.1016/j.ejmech.2013.10.017