Bicyclo[2.1.0]pentane-2-carboxylic acid, methyl ester, (1-alpha-,2-alpha-,4-alpha-)- (9CI)

Base Information

Chemical Name:Bicyclo[2.1.0]pentane-2-carboxylic acid, methyl ester, (1-alpha-,2-alpha-,4-alpha-)- (9CI)
CAS No.:105017-03-6
Molecular Formula:C₇H₁₀O₂
Molecular Weight:126.155
Hs Code.:
Mol file:105017-03-6.mol

Synonyms:Bicyclo[2.1.0]pentane-2-carboxylic acid, methyl ester, (1-alpha-,2-alpha-,4-alpha-)- (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Bicyclo[2.1.0]pentane-2-carboxylic acid, methyl ester, (1-alpha-,2-alpha-,4-alpha-)- (9CI)

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Technology Process of Bicyclo[2.1.0]pentane-2-carboxylic acid, methyl ester, (1-alpha-,2-alpha-,4-alpha-)- (9CI)

There total 11 articles about Bicyclo[2.1.0]pentane-2-carboxylic acid, methyl ester, (1-alpha-,2-alpha-,4-alpha-)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 67-56-1
methanol

: 24810-45-5
3-diazobicyclo-[3.1.0]hexan-2-one

: 24813-72-7,105017-03-6
bicyclo[2.1.0]pentane-2-carboxylic acid methyl ester

Guidance literature:: at 0 ℃; for 3h; Irradiation;
DOI:10.1021/jo970980e

Reference yield:

: 4160-49-0
bicyclo[3.1.0]hexan-2-one

: 24813-72-7,105017-03-6
bicyclo[2.1.0]pentane-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / 36 h / 70 °C

2: 0.40 g / TsN₃ / CH₂Cl₂ / 72 h

3: 90 percent / 3 h / 0 °C / Irradiation

With 4-toluenesulfonyl azide; In dichloromethane;
DOI:10.1021/jo970980e

Reference yield:

: 202812-59-7
3-[1-Dimethylamino-meth-(E)-ylidene]-bicyclo[3.1.0]hexan-2-one

: 24813-72-7,105017-03-6
bicyclo[2.1.0]pentane-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 0.40 g / TsN₃ / CH₂Cl₂ / 72 h

2: 90 percent / 3 h / 0 °C / Irradiation

With 4-toluenesulfonyl azide; In dichloromethane;
DOI:10.1021/jo970980e