VANADYL 2 11 20 29-TETRA-TERT-BUTYL-2 3&

Base Information

• Chemical Name: VANADYL 2 11 20 29-TETRA-TERT-BUTYL-2 3&
• CAS No.: 105011-00-5
• Molecular Formula: C₆₄H₅₆N₈OV
• Molecular Weight: 1004.14
• Mol file: 105011-00-5.mol

Synonyms:Vanadium,oxo[2,11,20,29-tetrakis(1,1-dimethylethyl)-37H,39H-tetranaphtho[2,3-b:2',3'-g:2'',3''-l:2''',3'''-q]porphyrazinato(2-)-N37,N38,N39,N40]-,(SP-5-12)-;37H,39H-Tetranaphtho[2,3-b:2',3'-g:2'',3''-l:2''',3'''-q]porphyrazine,2,11,20,29-tetrakis(1,1-dimethylethyl)-, vanadium complex;45H,47H-Tetraanthra[2,3-b:2',3'-g:2'',3''-l:2''',3'''-q]porphyrazine, vanadiumderiv.; Vanadyl 2,11,20,29-tetra-tert-butyl-2,3-naphthalocyanine

Chemical Property of VANADYL 2 11 20 29-TETRA-TERT-BUTYL-2 3&

Chemical Property:

• Melting Point: >300 °C(lit.)
• PSA: 114.71000
• LogP: 18.44830

Purity/Quality:

98%,99%, ^*data from raw suppliers

Vanadyl 2,11,20,29-tetra-tert-butyl-2,3-naphthalocyanine Dye content 95 % ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of VANADYL 2 11 20 29-TETRA-TERT-BUTYL-2 3&

There total 1 articles about VANADYL 2 11 20 29-TETRA-TERT-BUTYL-2 3& which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-tert-butylnaphthalene-2,3-dicarbonitrile (32703-82-5) + vanadium(III) chloride (7718-98-1) → tetra-{2,3-(6-tert-butyl)naphtho}-tetraazaporphinatooxyvanadium (105011-00-5)

Guidance literature:

With urea; In neat (no solvent); heating (220-230°C, within 1.5 h, N2 atmosphere), heating (220-230°C, 3 h), cooling; extn. (1.cyclohexane, 2.CHCl3), evapn. (vac.), treatment with dild. NaOH (10 min, 60°C), filtn., washing (H2O and dild. HCl), washing (H2O), dissolution (CHCl3), chromy. (Al2O3, CHCl3), evapn., heating (vac., 150-200°C); elem. anal.;

DOI:10.1007/BF00810897

upstream raw materials:

6-tert-butylnaphthalene-2,3-dicarbonitrile

vanadium(III) chloride