cis-1,2,3,4-tetrahydro-2,3-diphenylquinoxaline

Base Information

Chemical Name:cis-1,2,3,4-tetrahydro-2,3-diphenylquinoxaline
CAS No.:7739-06-2
Molecular Formula:C₂₀H₁₈N₂
Molecular Weight:286.376
Hs Code.:

Synonyms:cis-1,2,3,4-tetrahydro-2,3-diphenylquinoxaline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-1,2,3,4-tetrahydro-2,3-diphenylquinoxaline

Chemical Property:

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Technology Process of cis-1,2,3,4-tetrahydro-2,3-diphenylquinoxaline

There total 16 articles about cis-1,2,3,4-tetrahydro-2,3-diphenylquinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1684-14-6
2,3-diphenylquinoxaline

: 7739-06-2
cis-1,2,3,4-tetrahydro-2,3-diphenylquinoxaline

Guidance literature:: With tris(pentafluorophenyl)borate; hydrogen; In toluene; at 100 ℃; for 24h; under 15001.5 Torr; Reagent/catalyst; Temperature; diastereoselective reaction;
DOI:10.1002/anie.201409471

Reference yield:

: 91-19-0
2,3-diethynylquinoxaline

: phenylmagnesium bromide

: 7739-06-2,7739-07-3,75960-39-3,108839-24-3
(+/-)-trans-2,3-diphenyl-1,2,3,4-tetrahydro-quinoxaline

Guidance literature:: With diethyl ether; Behandeln des Reaktionsprodukts mit fluessigem NH₃;
DOI:10.1021/ja01352a034

Reference yield:

: 1684-14-6
2,3-diphenylquinoxaline

: 7739-06-2,7739-07-3,75960-39-3,108839-24-3
trans-1,2,3,4-tetrahydro-2,3-diphenylquinoxaline

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / titanium(III) chloride / ethanol / 18 h / Ambient temperature

2: titanium(III) chloride / ethanol / 18 h / Ambient temperature

With titanium(III) chloride; In ethanol;