2,2-difluoro-1-(4-methoxyphenyl)-2-phenylsulfanyl-1-trimethoxysiloxyethane

Base Information

• Chemical Name: 2,2-difluoro-1-(4-methoxyphenyl)-2-phenylsulfanyl-1-trimethoxysiloxyethane
• CAS No.: 899820-36-1
• Molecular Formula: C₁₈H₂₂F₂O₂SSi
• Molecular Weight: 368.52

Synonyms:2,2-difluoro-1-(4-methoxyphenyl)-2-phenylsulfanyl-1-trimethoxysiloxyethane

Chemical Property of 2,2-difluoro-1-(4-methoxyphenyl)-2-phenylsulfanyl-1-trimethoxysiloxyethane

Chemical Property:

Purity/Quality:

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Technology Process of 2,2-difluoro-1-(4-methoxyphenyl)-2-phenylsulfanyl-1-trimethoxysiloxyethane

There total 1 articles about 2,2-difluoro-1-(4-methoxyphenyl)-2-phenylsulfanyl-1-trimethoxysiloxyethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

4-methoxy-benzaldehyde (123-11-5) + phenyl (trimethylsilyl)difluoromethyl sulfide (536975-49-2) → 2,2-difluoro-1-(4-methoxyphenyl)-2-(phenylthio)ethan-1-ol (899820-35-0) + 2,2-difluoro-1-(4-methoxyphenyl)-2-phenylsulfanyl-1-trimethoxysiloxyethane (899820-36-1)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -78 - 20 ℃;

DOI:10.1016/j.tet.2006.04.015

Reference yield: 91.0%

2,2-difluoro-1-(4-methoxyphenyl)-2-phenylsulfanyl-1-trimethoxysiloxyethane (899820-36-1) → 2,2-difluoro-1-(4-methoxyphenyl)-2-(phenylthio)ethan-1-ol (899820-35-0)

Guidance literature:

With potassium fluoride; In dichloromethane; acetonitrile; at 20 ℃;

DOI:10.1016/j.tet.2006.04.015

Reference yield:

2,2-difluoro-1-(4-methoxyphenyl)-2-phenylsulfanyl-1-trimethoxysiloxyethane (899820-36-1) → C18H22F2O3SSi (1337571-98-8)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; at -78 - 20 ℃; for 12h;

DOI:10.1016/j.jfluchem.2011.06.036

upstream raw materials:

4-methoxy-benzaldehyde

phenyl (trimethylsilyl)difluoromethyl sulfide

Downstream raw materials:

2,2-difluoro-1-(4-methoxyphenyl)-2-(phenylthio)ethan-1-ol

C₁₈H₂₂F₂O₃SSi

ω,ω-Difluoro-4-methoxyacetophenone

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