1-amino-4-((tert-butyldimethylsilyloxy)methyl)pyridinium 2,4-dinitrophenolate

Base Information

Chemical Name:1-amino-4-((tert-butyldimethylsilyloxy)methyl)pyridinium 2,4-dinitrophenolate
CAS No.:1313726-18-9
Molecular Formula:C₆H₃N₂O₅*C₁₂H₂₃N₂OSi
Molecular Weight:422.513
Hs Code.:

Synonyms:1-amino-4-((tert-butyldimethylsilyloxy)methyl)pyridinium 2,4-dinitrophenolate

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Chemical Property of 1-amino-4-((tert-butyldimethylsilyloxy)methyl)pyridinium 2,4-dinitrophenolate

Chemical Property:

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Technology Process of 1-amino-4-((tert-butyldimethylsilyloxy)methyl)pyridinium 2,4-dinitrophenolate

There total 5 articles about 1-amino-4-((tert-butyldimethylsilyloxy)methyl)pyridinium 2,4-dinitrophenolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 117423-41-3
4-((tert-butyldimethylsilyloxy)methyl)pyridine

: 17508-17-7
O-(2,4-dinitrophenyl)hydroxylamine

: 1313726-18-9
1-amino-4-((tert-butyldimethylsilyloxy)methyl)pyridinium 2,4-dinitrophenolate

Guidance literature:: In acetonitrile; at 40 ℃; for 24h;

Reference yield:

: 584-48-5
2,4-dinitrobromobenzene

: 1313726-18-9
1-amino-4-((tert-butyldimethylsilyloxy)methyl)pyridinium 2,4-dinitrophenolate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / acetone / 3 h / 20 °C

2: hydrazine hydrate / dichloromethane; methanol / 6 h / 0 °C

3: acetonitrile / 24 h / 40 °C

With hydrazine hydrate; triethylamine; In methanol; dichloromethane; acetone; acetonitrile;

Reference yield:

: 586-95-8
pyridine-4-methanol

: 1313726-18-9
1-amino-4-((tert-butyldimethylsilyloxy)methyl)pyridinium 2,4-dinitrophenolate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 4 h / 0 - 20 °C

2: acetonitrile / 24 h / 40 °C

With triethylamine; In dichloromethane; acetonitrile;