C₃₀H₃₆N₄O₄

Base Information

Chemical Name:C₃₀H₃₆N₄O₄
CAS No.:1366595-53-0
Molecular Formula:C₃₀H₃₆N₄O₄
Molecular Weight:516.64
Hs Code.:

C<sub>30</sub>H<sub>36</sub>N<sub>4</sub>O<sub>4</sub>

Synonyms:C₃₀H₃₆N₄O₄

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Chemical Property of C₃₀H₃₆N₄O₄

Chemical Property:

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Technology Process of C₃₀H₃₆N₄O₄

There total 5 articles about C₃₀H₃₆N₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1366595-52-9
C₃₀H₃₉N₃O₇S

: 10442-39-4
tetra-n-butylammonium cyanide

: 1366595-53-0
C₃₀H₃₆N₄O₄

Guidance literature:: In N,N-dimethyl-formamide; at 80 ℃; for 2h; Inert atmosphere; Microwave irradiation;
DOI:10.1016/j.bmcl.2012.01.098

Reference yield:

: 851544-48-4
(3aS,5R,7aS,9aS)-3-benzyl-4-oxo-decahydro-2-oxa-3,4a-diazacyclopenta[f]azulene-5-carboxylic acid tert-butyl ester

: 1366595-53-0
C₃₀H₃₆N₄O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylsilane; trifluoroacetic acid / dichloromethane / 4 h / 20 °C

2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / Inert atmosphere

2.2: 18 h / 20 °C / Inert atmosphere

3.1: palladium on activated charcoal; hydrogen / ethanol; water / 3 h / 85 °C / 7500.75 Torr

4.1: triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

5.1: triethylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

6.1: N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere; Microwave irradiation

With triethylsilane; palladium on activated charcoal; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.01.098

Reference yield:

: 1366595-48-3
C₁₈H₂₂N₂O₄

: 1366595-53-0
C₃₀H₃₆N₄O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h / Inert atmosphere

1.2: 18 h / 20 °C / Inert atmosphere

2.1: palladium on activated charcoal; hydrogen / ethanol; water / 3 h / 85 °C / 7500.75 Torr

3.1: triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

4.1: triethylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

5.1: N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere; Microwave irradiation

With palladium on activated charcoal; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.01.098