2,2'-ethylenebis<2,5-dimethoxybenzyl alcohol> bis(hydrogen succinate)

Base Information

Chemical Name:2,2'-ethylenebis<2,5-dimethoxybenzyl alcohol> bis(hydrogen succinate)
CAS No.:120475-74-3
Molecular Formula:C₂₈H₃₄O₁₂
Molecular Weight:562.571
Hs Code.:

Synonyms:2,2'-ethylenebis<2,5-dimethoxybenzyl alcohol> bis(hydrogen succinate)

Suppliers and Price of 2,2'-ethylenebis<2,5-dimethoxybenzyl alcohol> bis(hydrogen succinate)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,2'-ethylenebis<2,5-dimethoxybenzyl alcohol> bis(hydrogen succinate)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,2'-ethylenebis<2,5-dimethoxybenzyl alcohol> bis(hydrogen succinate)

There total 5 articles about 2,2'-ethylenebis<2,5-dimethoxybenzyl alcohol> bis(hydrogen succinate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 108-30-5
succinic acid anhydride

: 120475-76-5
1,2-bis<4-(hydroxymethyl)-2,5-dimethoxyphenyl>ethane

: 120475-74-3
2,2'-ethylenebis<2,5-dimethoxybenzyl alcohol> bis(hydrogen succinate)

Guidance literature:: With dmap; triethylamine; In 1,4-dioxane; for 24h; Ambient temperature;
DOI:10.1021/jm00127a039

Reference yield:

: 120475-77-6
(Z)-1,2-bis<4-(acetoxymethyl)-2,5-dimethoxyphenyl>ethene

: 120475-74-3
2,2'-ethylenebis<2,5-dimethoxybenzyl alcohol> bis(hydrogen succinate)

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / H₂ / PtO₂ / acetic acid / 6 h / 2068.6 Torr

2: 82 percent / NaOH / methanol; tetrahydrofuran; H₂O / Ambient temperature

3: 87 percent / Et₃N, 4-(dimethylamino)pyridine / dioxane / 24 h / Ambient temperature

With dmap; sodium hydroxide; hydrogen; triethylamine; platinum(IV) oxide; In tetrahydrofuran; 1,4-dioxane; methanol; water; acetic acid;
DOI:10.1021/jm00127a039

Reference yield:

: 20306-76-7
2,5,2',5'-tetramethoxy-bibenzyl

: 120475-74-3
2,2'-ethylenebis<2,5-dimethoxybenzyl alcohol> bis(hydrogen succinate)

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / HCl-gas, conc. HCl / dioxane / 0.02 h

2: 81 percent / Na₂CO₃ / dioxane; H₂O / 8 h / Heating

3: 87 percent / Et₃N, 4-(dimethylamino)pyridine / dioxane / 24 h / Ambient temperature

With hydrogenchloride; dmap; sodium carbonate; triethylamine; In 1,4-dioxane; water;
DOI:10.1021/jm00127a039