2,2,3,3-Tetramethyl-cyclopropanecarboxylic acid 4-(2-benzyloxycarbonyl-ethyl)-phenyl ester

Base Information

Chemical Name:2,2,3,3-Tetramethyl-cyclopropanecarboxylic acid 4-(2-benzyloxycarbonyl-ethyl)-phenyl ester
CAS No.:208251-92-7
Molecular Formula:C₂₄H₂₈O₄
Molecular Weight:380.484
Hs Code.:

Synonyms:2,2,3,3-Tetramethyl-cyclopropanecarboxylic acid 4-(2-benzyloxycarbonyl-ethyl)-phenyl ester

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Chemical Property of 2,2,3,3-Tetramethyl-cyclopropanecarboxylic acid 4-(2-benzyloxycarbonyl-ethyl)-phenyl ester

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Technology Process of 2,2,3,3-Tetramethyl-cyclopropanecarboxylic acid 4-(2-benzyloxycarbonyl-ethyl)-phenyl ester

There total 3 articles about 2,2,3,3-Tetramethyl-cyclopropanecarboxylic acid 4-(2-benzyloxycarbonyl-ethyl)-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31770-76-0
3-(4-hydroxyphenyl)propionic acid benzyl ester

: 24303-61-5
2,2,3,3-tetramethylcyclopropanecarbonyl chloride

: 208251-92-7
2,2,3,3-Tetramethyl-cyclopropanecarboxylic acid 4-(2-benzyloxycarbonyl-ethyl)-phenyl ester

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃; for 0.5h;
DOI:10.1021/jf9710847

Reference yield:

: 501-97-3
4-hydroxyphenylpropionic acid

: 208251-92-7
2,2,3,3-Tetramethyl-cyclopropanecarboxylic acid 4-(2-benzyloxycarbonyl-ethyl)-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85percent aq. H₃PO₄ / toluene / 10 h / Heating

2: pyridine / CH₂Cl₂ / 0.5 h / 0 - 20 °C

With pyridine; phosphoric acid; In dichloromethane; toluene;
DOI:10.1021/jf9710847

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 208251-92-7
2,2,3,3-Tetramethyl-cyclopropanecarboxylic acid 4-(2-benzyloxycarbonyl-ethyl)-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85percent aq. H₃PO₄ / toluene / 10 h / Heating

2: pyridine / CH₂Cl₂ / 0.5 h / 0 - 20 °C

With pyridine; phosphoric acid; In dichloromethane; toluene;
DOI:10.1021/jf9710847