(2S)-2-[(4-methoxybenzyl)oxy]propanal O-[tert-butyl(dimethyl)silyl]oxime

Base Information

Chemical Name:(2S)-2-[(4-methoxybenzyl)oxy]propanal O-[tert-butyl(dimethyl)silyl]oxime
CAS No.:861902-98-9
Molecular Formula:C₁₇H₂₉NO₃Si
Molecular Weight:323.508
Hs Code.:

Synonyms:(2S)-2-[(4-methoxybenzyl)oxy]propanal O-[tert-butyl(dimethyl)silyl]oxime

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Chemical Property of (2S)-2-[(4-methoxybenzyl)oxy]propanal O-[tert-butyl(dimethyl)silyl]oxime

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Technology Process of (2S)-2-[(4-methoxybenzyl)oxy]propanal O-[tert-butyl(dimethyl)silyl]oxime

There total 2 articles about (2S)-2-[(4-methoxybenzyl)oxy]propanal O-[tert-butyl(dimethyl)silyl]oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 41879-39-4
O-(tert-butyldimethylsilanyl)hydroxylamine

: 126361-27-1
(S)-(p-methoxybenzyloxy)propanal

: 861902-98-9
(2S)-2-[(4-methoxybenzyl)oxy]propanal O-[tert-butyl(dimethyl)silyl]oxime

Guidance literature:: With 4 A molecular sieve; In chloroform; at 20 ℃; for 12h;
DOI:10.1021/ol0508429

Reference yield: 86.0%

: 126361-27-1
(S)-(p-methoxybenzyloxy)propanal

: 861902-98-9
(2S)-2-[(4-methoxybenzyl)oxy]propanal O-[tert-butyl(dimethyl)silyl]oxime

Guidance literature:: With O-(tert-butyldimethylsilanyl)hydroxylamine; In chloroform; at 20 ℃; for 12h; Molecular sieve;
DOI:10.1021/jo8016692

Reference yield:

: 861902-98-9
(2S)-2-[(4-methoxybenzyl)oxy]propanal O-[tert-butyl(dimethyl)silyl]oxime

: 861903-07-3
(1S)-2-([tert-butyl(dimethyl)silyl]oxyimino)-1-methylethyl (3S)-3-[(4-methoxybenzyl)oxy] butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: DDQ; phosphate buffer / CH₂Cl₂ / 1 h / 20 °C / pH 7.0

2: 1.7 g / EDCI; DMAP / CH₂Cl₂ / 12 h / 20 °C

With dmap; phosphate buffer; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane;
DOI:10.1021/ol0508429