(Z)-METHYL 2-ACETAMIDO-3-(4-CHLOROPHENYL)ACRYLATE

Base Information

Chemical Name:(Z)-METHYL 2-ACETAMIDO-3-(4-CHLOROPHENYL)ACRYLATE
CAS No.:102245-02-3
Molecular Formula:C12H12 Cl N O3
Molecular Weight:253.685
Hs Code.:
Mol file:102245-02-3.mol

Synonyms:2-Propenoicacid, 2-(acetylamino)-3-(4-chlorophenyl)-, methyl ester, (Z)-; (2Z)-2-(Acetylamino)-3-(4-chlorophenyl)-2-propenoicacid methyl ester; Methyl a-acetamido-4-chlorocinnamate

Suppliers and Price of (Z)-METHYL 2-ACETAMIDO-3-(4-CHLOROPHENYL)ACRYLATE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of (Z)-METHYL 2-ACETAMIDO-3-(4-CHLOROPHENYL)ACRYLATE

Chemical Property:

PSA：55.40000
LogP:2.38090

Purity/Quality:: 99%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (Z)-METHYL 2-ACETAMIDO-3-(4-CHLOROPHENYL)ACRYLATE

There total 14 articles about (Z)-METHYL 2-ACETAMIDO-3-(4-CHLOROPHENYL)ACRYLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 67-56-1
methanol

: 104-88-1
4-chlorobenzaldehyde

: 543-24-8
N-acetylglycine

: 102245-02-3
methyl (Z)-2-acetylamino-3-(4-chlorophenyl)-2-propenoate

Guidance literature:: N-acetylglycine; With chloroformic acid ethyl ester; triethylamine; In benzene; at 0 - 20 ℃;

4-chlorobenzaldehyde; In benzene; at 80 ℃; for 2h;

methanol; With triethylamine; at 65 ℃; for 3h;
DOI:10.1039/d0ob00557f

Reference yield: 70.0%

: 108-24-7
acetic anhydride

: 102244-86-0
(Z)-methyl 2-azido-3-(4-chlorophenyl)acrylate

: 102245-02-3
methyl (Z)-2-acetylamino-3-(4-chlorophenyl)-2-propenoate

: 102245-06-7
4-Chlor-α-amino-zimtsaeuremethylester

: 102244-94-0
4-Chlor-α-(N,N-diacetylamino-)-zimtsaeuremethylester

Guidance literature:: In acetonitrile; at 25 - 30 ℃; electrochemical;
DOI:10.1007/BF00811247

Reference yield: 62.0%

: 106-39-8
bromochlorobenzene

: 35356-70-8
Methyl 2-acetamidoacrylate

: 102245-02-3
methyl (Z)-2-acetylamino-3-(4-chlorophenyl)-2-propenoate

Guidance literature:: With benzyltriethylammonium bromide; N-ethyl-N,N-diisopropylamine; palladium diacetate; In 1-methyl-pyrrolidin-2-one; at 125 ℃; for 3h;
DOI:10.1016/j.jorganchem.2003.09.012