1-(3-pyridyl)-3-phenylbenzoquinoline

Base Information

• Chemical Name: 1-(3-pyridyl)-3-phenylbenzoquinoline
• CAS No.: 20856-18-2
• Molecular Formula: C₂₄H₁₆N₂
• Molecular Weight: 332.404

Synonyms:1-(3-pyridyl)-3-phenylbenzoquinoline

Chemical Property of 1-(3-pyridyl)-3-phenylbenzoquinoline

Chemical Property:

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Technology Process of 1-(3-pyridyl)-3-phenylbenzoquinoline

There total 3 articles about 1-(3-pyridyl)-3-phenylbenzoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

3-oxo-3-pyridin-3-yl-propionic acid ethyl ester (6283-81-4) + benzylidene(2-naphthyl)amine (891-32-7) → 1-(3-pyridyl)-3-phenylbenzoquinoline (20856-18-2)

Guidance literature:

With hydrogenchloride; In various solvent(s); at 100 - 150 ℃; for 2h;

DOI:10.1007/BF01164869

Reference yield:

(E)-N-(naphthalen-2-yl)-1-phenylmethanimine (75472-73-0) + 3-oxo-3-pyridin-3-yl-propionic acid ethyl ester (6283-81-4) → 1-(3-pyridyl)-3-phenylbenzoquinoline (20856-18-2)

Guidance literature:

With hydrogenchloride; In ethanol; water; at 100 ℃;

DOI:10.1134/S1070428007050119

Reference yield:

→ 1-(3-pyridyl)-3-phenylbenzoquinoline (20856-18-2)

Guidance literature:

entspr. N-Benzyliden-<2>naphthylamin, 3-Acetylpyridin;

upstream raw materials:

3-oxo-3-pyridin-3-yl-propionic acid ethyl ester

benzylidene(2-naphthyl)amine

(E)-N-(naphthalen-2-yl)-1-phenylmethanimine

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