Technology Process of C20H23FN4O2
There total 10 articles about C20H23FN4O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
iron; ammonium chloride;
In
tetrahydrofuran; methanol;
at 70 ℃;
for 1.5h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 0 °C
1.2: 1.5 h / 0 °C
2.1: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 / 1,4-dioxane / 18 h / 65 °C
3.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium carbonate / tetrahydrofuran; water / 14 h / 70 °C
4.1: trimethylaluminum; ammonium chloride / toluene / 26 h / 100 °C
5.1: sulfuric acid / 14.5 h / 20 °C
5.2: 1 h / 0 °C
6.1: tetrahydrofuran / 15 h / 20 °C
7.1: ammonium chloride; iron / methanol; tetrahydrofuran / 1.5 h / 70 °C
With
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; sulfuric acid; potassium tert-butylate; trimethylaluminum; potassium acetate; iron; potassium carbonate; ammonium chloride;
In
tetrahydrofuran; 1,4-dioxane; methanol; water; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sulfuric acid / 14.5 h / 20 °C
1.2: 1 h / 0 °C
2.1: tetrahydrofuran / 15 h / 20 °C
3.1: ammonium chloride; iron / methanol; tetrahydrofuran / 1.5 h / 70 °C
With
sulfuric acid; iron; ammonium chloride;
In
tetrahydrofuran; methanol;
