Re(N-2,6-C₆H₃Me₂)3Cl

Base Information

Chemical Name:Re(N-2,6-C₆H₃Me₂)3Cl
CAS No.:118968-23-3
Molecular Formula:C₂₄H₂₇ClN₃Re
Molecular Weight:579.158
Hs Code.:

Re(N-2,6-C<sub>6</sub>H<sub>3</sub>Me<sub>2</sub>)3Cl

Synonyms:Re(N-2,6-C₆H₃Me₂)3Cl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Re(N-2,6-C₆H₃Me₂)3Cl

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Technology Process of Re(N-2,6-C₆H₃Me₂)3Cl

There total 1 articles about Re(N-2,6-C₆H₃Me₂)3Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: {2,6-Me₂C₆H₃NH₃}{Re(N-2,6-Me₂C₆H₃)2Cl₄}

: 118968-23-3
Re(N-2,6-C₆H₃Me₂)3Cl

: 554-68-7
triethylamine hydrochloride

Guidance literature:: With triethylamine; In dichloromethane; at -20°C, warmed to 25°C over 30 min; removal of solvent in vac., extn. (pentane), filtered through Celite, reduced to dryness in vac., crystn. from pentane, good yield; elem. anal.;
DOI:10.1016/S0277-5387(00)80695-6

Reference yield: 80.0%

: 118968-23-3
Re(N-2,6-C₆H₃Me₂)3Cl

: 13132-23-5
2,2-dimethylpropylmagnesium chloride

: 118968-29-9
Re(N-2,6-C₆H₃Me₂)3(CH₂t-Bu)

Guidance literature:: In diethyl ether; byproducts: MgCl2; addn. of t-BuCH2MgCl in ether to a soln. of Re-compd. in ether at -40°C, stirred for 48 h at 25°C; filtered through Celite (removal of MgCl2), taken to dryness, extn. (pentane), filtered through Celite, concd., cooled, recrystn. (pentane); elem. anal.;
DOI:10.1016/S0277-5387(00)80695-6