bis(3-fluoro-2-(trimethylsilyl)phenyl)methoxyborane

Base Information

Chemical Name:bis(3-fluoro-2-(trimethylsilyl)phenyl)methoxyborane
CAS No.:1257793-02-4
Molecular Formula:C₁₉H₂₇BF₂OSi₂
Molecular Weight:376.402
Hs Code.:

Synonyms:bis(3-fluoro-2-(trimethylsilyl)phenyl)methoxyborane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(3-fluoro-2-(trimethylsilyl)phenyl)methoxyborane

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Technology Process of bis(3-fluoro-2-(trimethylsilyl)phenyl)methoxyborane

There total 1 articles about bis(3-fluoro-2-(trimethylsilyl)phenyl)methoxyborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 121-43-7,63156-11-6
Trimethyl borate

: 632324-41-5
1-bromo-3-fluoro-2-(trimethylsilyl)benzene

: (3-fluoro-2-(trimethylsilyl)phenyl)dimethoxyborane

: 1257793-02-4
bis(3-fluoro-2-(trimethylsilyl)phenyl)methoxyborane

Guidance literature:: 1-bromo-3-fluoro-2-(trimethylsilyl)benzene; With n-butyllithium; In tetrahydrofuran; diethyl ether; at -70 ℃; Inert atmosphere;

Trimethyl borate; In tetrahydrofuran; diethyl ether; at -60 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.jorganchem.2010.08.016

Reference yield: 58.0%

: 148-24-3,24804-14-6
8-quinolinol

: 1257793-02-4
bis(3-fluoro-2-(trimethylsilyl)phenyl)methoxyborane

: 7790-99-0
Iodine monochloride

: 1257793-18-2
bis(3-fluoro-2-iodophenyl)borinic acid 8-hydroxyquinolineester

Guidance literature:: In chloroform; (Ar); stirring mixt. of boronic acid deriv., 1.1 equiv. of ICl and CHCl3at reflux for 6 h, evapn., dissolving in diethyl ether, addn. of quinol ine deriv., stirring for 12 h; filtration, washing with diethyl ether and hexane, elem. anal.;
DOI:10.1016/j.jorganchem.2010.08.016