Benzene, 1-broMo-3-fluoro-2-(triMethylsilyl)-

Base Information

Chemical Name:Benzene, 1-broMo-3-fluoro-2-(triMethylsilyl)-
CAS No.:632324-41-5
Molecular Formula:C9H12BrFSi
Molecular Weight:247.182
Hs Code.:
Mol file:632324-41-5.mol

Synonyms:(2-bromo-6-fluorophenyl)(trimethyl)silane;(2-bromo-6-fluorophenyl)-(trimethyl)silane;

Suppliers and Price of Benzene, 1-broMo-3-fluoro-2-(triMethylsilyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AOBChem
1-Bromo-3-fluoro-2-(trimethylsilyl)benzene 97%
500mg
$ 183.00

ACHEMBLOCK
1-Bromo-3-fluoro-2-(trimethylsilyl)benzene 95%
5G
$ 1085.00

ACHEMBLOCK
1-Bromo-3-fluoro-2-(trimethylsilyl)benzene 95%
1G
$ 305.00

Total 5 raw suppliers

Chemical Property of Benzene, 1-broMo-3-fluoro-2-(triMethylsilyl)-

Chemical Property:

PSA：0.00000
LogP:3.13340

Purity/Quality:

99% ^*data from raw suppliers

1-Bromo-3-fluoro-2-(trimethylsilyl)benzene 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzene, 1-broMo-3-fluoro-2-(triMethylsilyl)-

There total 2 articles about Benzene, 1-broMo-3-fluoro-2-(triMethylsilyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 75-77-4
chloro-trimethyl-silane

: 1073-06-9
3-fluorobromobenzene

: 632324-41-5
1-bromo-3-fluoro-2-(trimethylsilyl)benzene

: 1-bromo-3-fluoro-2,4-bis(trimethylsilyl)benzene

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -75 ℃; for 0.5h;
DOI:10.1021/jo034790h

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 1073-06-9
3-fluorobromobenzene

: 632324-41-5
1-bromo-3-fluoro-2-(trimethylsilyl)benzene

Guidance literature:: chloro-trimethyl-silane; 3-fluorobromobenzene; With lithium diisopropyl amide; In tetrahydrofuran; at -70 ℃; for 1h;

With sulfuric acid; In tetrahydrofuran; water;

Reference yield: 80.0%

: 121-43-7,63156-11-6
Trimethyl borate

: 632324-41-5
1-bromo-3-fluoro-2-(trimethylsilyl)benzene

: 1257792-92-9
3-fluoro-2-(trimethylsilyl)phenylboronic acid

Guidance literature:: 1-bromo-3-fluoro-2-(trimethylsilyl)benzene; With n-butyllithium; In tetrahydrofuran; diethyl ether; at -75 ℃; for 0.5h; Inert atmosphere;

Trimethyl borate; In tetrahydrofuran; diethyl ether; at -90 ℃; Inert atmosphere;

With sulfuric acid; In tetrahydrofuran; diethyl ether; water;
DOI:10.1016/j.jorganchem.2010.08.016