4-CHLOROMETHYLSTILBENE

Base Information

• Chemical Name: 4-CHLOROMETHYLSTILBENE
• CAS No.: 101095-61-8
• Molecular Formula: C15H13 Cl
• Molecular Weight: 228.721
• Mol file: 101095-61-8.mol

Synonyms:Stilbene,4-(chloromethyl)- (6CI); 4-(Chloromethyl)stilbene; p-(Chloromethyl)stilbene

Chemical Property of 4-CHLOROMETHYLSTILBENE

Chemical Property:

• Boiling Point: 353.1±22.0 °C(Predicted)
• PSA: 0.00000
• Density: 1.141±0.06 g/cm3(Predicted)
• LogP: 4.59580

Purity/Quality:

98.5% ^*data from raw suppliers

4-CHLOROMETHYLSTILBENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-CHLOROMETHYLSTILBENE

There total 4 articles about 4-CHLOROMETHYLSTILBENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Vinylbenzyl chloride (1592-20-7,29296-32-0) + chlorobenzene (108-90-7) → 4-chloromethylstilbene (101095-61-8)

Guidance literature:

With C₂₈H₂₅N₅O₄PdS₂; potassium carbonate; In water; N,N-dimethyl-formamide; at 140 ℃; for 12h;

DOI:10.1016/j.molstruc.2019.127030

Reference yield:

bromobenzene (108-86-1,52753-63-6) + 4-Vinylbenzyl chloride (1592-20-7,29296-32-0) → 4-chloromethylstilbene (101095-61-8)

Guidance literature:

With C₂₈H₂₅N₅O₄PdS₂; potassium carbonate; In water; N,N-dimethyl-formamide; at 140 ℃; for 3h;

DOI:10.1016/j.molstruc.2019.127030

Reference yield:

<4-Styryl-benzyl>-dimethylamin (101583-54-4) → 4-chloromethylstilbene (101095-61-8)

Guidance literature:

With benzoyl chloride;

upstream raw materials:

4-chloromethylbenzaldehyde

benzyltriphenylphosphonium chloride

<4-Styryl-benzyl>-dimethylamin

4-Vinylbenzyl chloride

Downstream raw materials:

6-ethoxycarbonyl-2-methyl-1-[4-(2-phenylethenyl)benzyl]benzimidazole