2,6-d₂-4-fluorobromobenzene

Base Information

Chemical Name:2,6-d₂-4-fluorobromobenzene
CAS No.:1514866-09-1
Molecular Formula:C₆H₄BrF
Molecular Weight:176.984
Hs Code.:

Synonyms:2,6-d₂-4-fluorobromobenzene

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Chemical Property of 2,6-d₂-4-fluorobromobenzene

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Technology Process of 2,6-d₂-4-fluorobromobenzene

There total 2 articles about 2,6-d₂-4-fluorobromobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 2557-69-9
2,6-d₂-4-fluoroaniline

: 1514866-09-1
2,6-d₂-4-fluorobromobenzene

Guidance literature:: 2,6-d₂-4-fluoroaniline; With hydrogen bromide; In water; for 0.25h;

With sodium nitrite; In water; at 0 ℃; for 0.5h;

With copper(I) bromide; In water; at 50 ℃;
DOI:10.1021/ja408712e

Reference yield:

: 371-40-4
4-fluoroaniline

: 1514866-09-1
2,6-d₂-4-fluorobromobenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / diethyl ether / 0.25 h

1.2: 140 °C / Sealed tube

2.1: hydrogen bromide / water / 0.25 h

2.2: 0.5 h / 0 °C

2.3: 50 °C

With hydrogenchloride; hydrogen bromide; In diethyl ether; water;
DOI:10.1021/ja408712e

Reference yield: 60.0%

: 75-77-4
chloro-trimethyl-silane

: 1514866-09-1
2,6-d₂-4-fluorobromobenzene

: 1514864-11-9
(2,6-d₂-4-fluorophenyl)trimethylsilane

Guidance literature:: 2,6-d₂-4-fluorobromobenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

chloro-trimethyl-silane; In tetrahydrofuran; hexane; at 20 ℃;
DOI:10.1021/ja408712e