(3-Cyano-4-phenyl-6-thiophen-2-yl-pyridin-2-ylsulfanyl)-acetic acid [1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide

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Chemical Name:(3-Cyano-4-phenyl-6-thiophen-2-yl-pyridin-2-ylsulfanyl)-acetic acid [1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide
CAS No.:847976-33-4
Molecular Formula:C₂₆H₂₀N₄O₂S₂
Molecular Weight:484.602
Hs Code.:

Synonyms:(3-Cyano-4-phenyl-6-thiophen-2-yl-pyridin-2-ylsulfanyl)-acetic acid [1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide

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Chemical Property of (3-Cyano-4-phenyl-6-thiophen-2-yl-pyridin-2-ylsulfanyl)-acetic acid [1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide

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Technology Process of (3-Cyano-4-phenyl-6-thiophen-2-yl-pyridin-2-ylsulfanyl)-acetic acid [1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide

There total 4 articles about (3-Cyano-4-phenyl-6-thiophen-2-yl-pyridin-2-ylsulfanyl)-acetic acid [1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 123-11-5
4-methoxy-benzaldehyde

: 847976-24-3
(3-cyano-4-phenyl-6-thiophen-2-yl-pyridin-2-ylsulfanyl)-acetic acid hydrazide

: 847976-33-4
(3-Cyano-4-phenyl-6-thiophen-2-yl-pyridin-2-ylsulfanyl)-acetic acid [1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide

Guidance literature:: In ethanol; for 4h; Heating;
DOI:10.1080/10426500490467147

Reference yield:

: 3988-77-0,39078-33-6,69656-36-6
3-phenyl-1-thiophen-2-yl-propenone

: 847976-33-4
(3-Cyano-4-phenyl-6-thiophen-2-yl-pyridin-2-ylsulfanyl)-acetic acid [1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: 43 percent / piperidine / ethanol / 4 h / Heating

2: 95 percent / sodium acetate trihydrate / ethanol / 2 h / Heating

3: 86 percent / N₂H₄*H₂O / ethanol / 4 h / Heating

4: 98 percent / ethanol / 4 h / Heating

With piperidine; sodium acetate; hydrazine hydrate; In ethanol;
DOI:10.1080/10426500490467147

Reference yield:

: 82127-11-5
4-phenyl-6-(thiophen-2-yl)-2-thioxo-1,2-dihydropyridine-3-carbonitrile

: 847976-33-4
(3-Cyano-4-phenyl-6-thiophen-2-yl-pyridin-2-ylsulfanyl)-acetic acid [1-(4-methoxy-phenyl)-meth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / sodium acetate trihydrate / ethanol / 2 h / Heating

2: 86 percent / N₂H₄*H₂O / ethanol / 4 h / Heating

3: 98 percent / ethanol / 4 h / Heating

With sodium acetate; hydrazine hydrate; In ethanol;
DOI:10.1080/10426500490467147