1H,1H,10H,10H-perfluorodecane-1,10-diyl bis[4-(trifluorovinyloxy)benzoate]

Base Information

Chemical Name:1H,1H,10H,10H-perfluorodecane-1,10-diyl bis[4-(trifluorovinyloxy)benzoate]
CAS No.:741700-79-8
Molecular Formula:C₂₈H₁₂F₂₂O₆
Molecular Weight:862.365
Hs Code.:

Synonyms:1H,1H,10H,10H-perfluorodecane-1,10-diyl bis[4-(trifluorovinyloxy)benzoate]

Suppliers and Price of 1H,1H,10H,10H-perfluorodecane-1,10-diyl bis[4-(trifluorovinyloxy)benzoate]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H,1H,10H,10H-perfluorodecane-1,10-diyl bis[4-(trifluorovinyloxy)benzoate]

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Technology Process of 1H,1H,10H,10H-perfluorodecane-1,10-diyl bis[4-(trifluorovinyloxy)benzoate]

There total 2 articles about 1H,1H,10H,10H-perfluorodecane-1,10-diyl bis[4-(trifluorovinyloxy)benzoate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9-hexadecafluorodecane-1,10-diol: 754-96-1
2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9-hexadecafluorodecane-1,10-diol

: 134151-66-9
4-(trifluorovinyloxy)benzoic acid

: 741700-79-8
1H,1H,10H,10H-perfluorodecane-1,10-diyl bis[4-(trifluorovinyloxy)benzoate]

Guidance literature:: With dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate; In dichloromethane; for 25h;
DOI:10.1021/ma049783p

Reference yield:

: 134151-77-2
1-bromo-4-(trifluorovinyloxy)benzene

: 741700-79-8
1H,1H,10H,10H-perfluorodecane-1,10-diyl bis[4-(trifluorovinyloxy)benzoate]

Guidance literature:: Multi-step reaction with 2 steps

1.1: tert-butyllithium / diethyl ether; pentane / -78 °C

1.2: 63 percent / diethyl ether; pentane / 1.25 h / -78 - 20 °C

2.1: 87 percent / 4-(dimethylamino)pyridinium 4-toluenesulfonate; N,N'-dicyclohexylcarbodiimide / CH₂Cl₂ / 25 h

With tert.-butyl lithium; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate; In diethyl ether; dichloromethane; pentane;
DOI:10.1021/ma049783p