1H,1H,10H,10H-Perfluorodecane-1,10-diol

Base Information

Chemical Name:1H,1H,10H,10H-Perfluorodecane-1,10-diol
CAS No.:754-96-1
Molecular Formula:C10H6F16O2
Molecular Weight:462.131
Hs Code.:29055900
European Community (EC) Number:670-426-5
DSSTox Substance ID:DTXSID50369896
Nikkaji Number:J940.872J
Wikidata:Q81985740
Mol file:754-96-1.mol

Synonyms:1H,1H,10H,10H-perfluorodecane-1,10-diol;FC10diol

Suppliers and Price of 1H,1H,10H,10H-Perfluorodecane-1,10-diol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
1H,1H,10H,10H-Perfluoro-1,10-decanediol
100mg
$ 60.00

TCI Chemical
1H,1H,10H,10H-Hexadecafluoro-1,10-decanediol >97.0%(GC)
5g
$ 70.00

TCI Chemical
1H,1H,10H,10H-Hexadecafluoro-1,10-decanediol >97.0%(GC)
1g
$ 26.00

SynQuest Laboratories
1H,1H,10H,10H-Perfluoro-1,10-decanediol 96%
5 g
$ 30.00

SynQuest Laboratories
1H,1H,10H,10H-Perfluoro-1,10-decanediol 96%
2 g
$ 15.00

SynQuest Laboratories
1H,1H,10H,10H-Perfluoro-1,10-decanediol 96%
25 g
$ 95.00

Sigma-Aldrich
2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9-Hexadecafluoro-1,10-decanediol 97%
5g
$ 77.20

Oakwood
1H,1H,10H,10H-Perfluorodecane-1,10-diol
5g
$ 30.00

Oakwood
1H,1H,10H,10H-Perfluorodecane-1,10-diol
1g
$ 15.00

Matrix Scientific
1H,1H,10H,10H-Perfluorodecane-1,10-diol 96%
25g
$ 135.00

Total 35 raw suppliers

Chemical Property of 1H,1H,10H,10H-Perfluorodecane-1,10-diol

Chemical Property:

Appearance/Colour:white powder and chunks
Vapor Pressure:0.000868mmHg at 25°C
Melting Point:135-137 °C(lit.)
Refractive Index:1.313
Boiling Point:271 °C at 760 mmHg
Flash Point:117.7 °C
PSA：40.46000
Density:1.673 g/cm³
LogP:4.05340
XLogP3:4.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:18
Rotatable Bond Count:9
Exact Mass:462.0112300
Heavy Atom Count:28
Complexity:518

Purity/Quality:

97% ^*data from raw suppliers

1H,1H,10H,10H-Perfluoro-1,10-decanediol ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 37/39-26-24/25

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C(C(C(C(C(C(C(C(C(CO)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)(F)F)O
Uses 2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9-Hexadecafluoro-1,10-decanediol may be used in the preparation of diverse bromo(ester) (macro)initiators, required for the preparation of fluorinated pentablock as well as amphiphilic triblock copolymers with a central polyether segment.

Technology Process of 1H,1H,10H,10H-Perfluorodecane-1,10-diol

There total 2 articles about 1H,1H,10H,10H-Perfluorodecane-1,10-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 423-91-6
diethyl perfluorosebacate

2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9-hexadecafluorodecane-1,10-diol: 754-96-1
2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9-hexadecafluorodecane-1,10-diol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; 0 deg C, 1 h, reflux, 12 h;
DOI:10.1016/S0022-2860(98)00797-2

Reference yield:

: 307-78-8
perfluorosebacic acid

2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9-hexadecafluorodecane-1,10-diol: 754-96-1
2,2,3,3,4,4,5,5,6,6,7,7,8,8,9,9-hexadecafluorodecane-1,10-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / conc.H₂SO₄ / 24 h / Heating

2: 90 percent / LiAlH₄ / tetrahydrofuran / 0 deg C, 1 h, reflux, 12 h

With lithium aluminium tetrahydride; sulfuric acid; In tetrahydrofuran;
DOI:10.1016/S0022-2860(98)00797-2