cyclopropylcarbamic acid 4-nitrophenyl ester

Base Information

• Chemical Name: cyclopropylcarbamic acid 4-nitrophenyl ester
• CAS No.: 444288-42-0
• Molecular Formula: C₁₀H₁₀N₂O₄
• Molecular Weight: 222.2
• Mol file: 444288-42-0.mol

Synonyms:cyclopropylcarbamic acid 4-nitrophenyl ester

Chemical Property of cyclopropylcarbamic acid 4-nitrophenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cyclopropylcarbamic acid 4-nitrophenyl ester

There total 3 articles about cyclopropylcarbamic acid 4-nitrophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

4-Nitrophenyl chloroformate (7693-46-1) + Cyclopropylamine (765-30-0) → cyclopropylcarbamic acid 4-nitrophenyl ester (444288-42-0)

Guidance literature:

In acetonitrile; at 0 - 20 ℃; for 24h; Solvent; Temperature;

DOI:10.1007/s11696-020-01402-z

Reference yield:

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) → cyclopropylcarbamic acid 4-nitrophenyl ester (444288-42-0)

Guidance literature:

Multi-step reaction with 2 steps

1: N,N-diethylaniline / toluene / 1 h / 0 °C

2: acetonitrile / 24 h / 0 - 20 °C

With N,N-diethylaniline; In toluene; acetonitrile;

DOI:10.1007/s11696-020-01402-z

Reference yield:

→ cyclopropylcarbamic acid 4-nitrophenyl ester (444288-42-0)

Guidance literature:

upstream raw materials:

4-Nitrophenyl chloroformate

Cyclopropylamine

4-nitro-phenol

Downstream raw materials:

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