ethyl 3-[(4-dipropylaminobutyl)(4-{[(1H-imidazol-2-ylmethyl)(1-methyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyl)amino]propionate

Base Information

Chemical Name:ethyl 3-[(4-dipropylaminobutyl)(4-{[(1H-imidazol-2-ylmethyl)(1-methyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyl)amino]propionate
CAS No.:864911-42-2
Molecular Formula:C₃₂H₅₁N₇O₂
Molecular Weight:565.803
Hs Code.:

Synonyms:ethyl 3-[(4-dipropylaminobutyl)(4-{[(1H-imidazol-2-ylmethyl)(1-methyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyl)amino]propionate

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Chemical Property of ethyl 3-[(4-dipropylaminobutyl)(4-{[(1H-imidazol-2-ylmethyl)(1-methyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyl)amino]propionate

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Technology Process of ethyl 3-[(4-dipropylaminobutyl)(4-{[(1H-imidazol-2-ylmethyl)(1-methyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyl)amino]propionate

There total 6 articles about ethyl 3-[(4-dipropylaminobutyl)(4-{[(1H-imidazol-2-ylmethyl)(1-methyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyl)amino]propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-[(4-dipropylamino-butyl)-(4-{[(1H-imidazol-2-ylmethyl)-(1-methyl-1H-imidazol-2-ylmethyl)-amino]-methyl}-benzyl)-amino]-propionic acid hydrochloride

: 64-17-5
ethanol

: 864911-42-2
ethyl 3-[(4-dipropylaminobutyl)(4-{[(1H-imidazol-2-ylmethyl)(1-methyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyl)amino]propionate

Guidance literature:: for 16h; Heating / reflux;

Reference yield:

: 927885-21-0
N-{4-[(benzylideneamino)methyl]benzyl}-N',N'-dipropylbutane-1,4-diamine

: 864911-42-2
ethyl 3-[(4-dipropylaminobutyl)(4-{[(1H-imidazol-2-ylmethyl)(1-methyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyl)amino]propionate

Guidance literature:: Multi-step reaction with 4 steps

1.1: ytterbium trifluoromethanesulfonate / acetonitrile; toluene / 92 h / 20 °C / Inert atmosphere

2.1: hydrogenchloride / ethanol / 5.5 h / 20 °C / Cooling with ice

2.2: pH 9

3.1: trimethyl orthoformate / ethanol / 19 h / 20 °C

3.2: 2 h / 20 °C / Cooling with ice

4.1: sodium tris(acetoxy)borohydride; ethanol / ethanol / 72 h / 20 °C

4.2: 2 h / 20 °C / Cooling with ice

With hydrogenchloride; ytterbium trifluoromethanesulfonate; ethanol; sodium tris(acetoxy)borohydride; trimethyl orthoformate; In ethanol; toluene; acetonitrile;

Reference yield:

: 1370602-25-7
ethyl 3-[(4-aminomethylbenzyl)(4-dipropylaminobutyl)amino]propionate

: 864911-42-2
ethyl 3-[(4-dipropylaminobutyl)(4-{[(1H-imidazol-2-ylmethyl)(1-methyl-1H-imidazol-2-ylmethyl)amino]methyl}benzyl)amino]propionate

Guidance literature:: Multi-step reaction with 2 steps

1.1: trimethyl orthoformate / ethanol / 19 h / 20 °C

1.2: 2 h / 20 °C / Cooling with ice

2.1: sodium tris(acetoxy)borohydride; ethanol / ethanol / 72 h / 20 °C

2.2: 2 h / 20 °C / Cooling with ice

With ethanol; sodium tris(acetoxy)borohydride; trimethyl orthoformate; In ethanol;