C₁₁H₁₀O₃

Base Information

Chemical Name:C₁₁H₁₀O₃
CAS No.:33121-49-2
Molecular Formula:C₁₁H₁₀O₃
Molecular Weight:190.199
Hs Code.:

C<sub>11</sub>H<sub>10</sub>O<sub>3</sub>

Synonyms:C₁₁H₁₀O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₁H₁₀O₃

Chemical Property:

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Technology Process of C₁₁H₁₀O₃

There total 5 articles about C₁₁H₁₀O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 549546-05-6
C₁₃H₁₂O₄

: 33121-49-2
C₁₁H₁₀O₃

Guidance literature:: With methanol; acetyl chloride; at 23 - 50 ℃; Inert atmosphere;
DOI:10.1021/jo501302f

Reference yield:

: 37167-62-7,3042-81-7,61139-20-6
bromo-phenyl-acetic acid methyl ester

: 33121-49-2
C₁₁H₁₀O₃

Guidance literature:: Multi-step reaction with 5 steps

1: 4 h / 160 °C

2: potassium hydroxide / ethanol; water / 5 h / 23 °C

3: triethylamine; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 3 h / 0 - 23 °C

4: lithium hexamethyldisilazane / tetrahydrofuran / 14 h / -78 - 23 °C / Inert atmosphere

5: acetyl chloride; methanol / 23 - 50 °C / Inert atmosphere

With methanol; tetra-(n-butyl)ammonium iodide; triethylamine; acetyl chloride; potassium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; ethanol; water; N,N-dimethyl-formamide; 1: |Arbuzov Reaction / 4: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1021/jo501302f

Reference yield:

: 38654-91-0
2-(diethoxyphosphino)-2-phenylacetic acid

: 33121-49-2
C₁₁H₁₀O₃

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 3 h / 0 - 23 °C

2: lithium hexamethyldisilazane / tetrahydrofuran / 14 h / -78 - 23 °C / Inert atmosphere

3: acetyl chloride; methanol / 23 - 50 °C / Inert atmosphere

With methanol; tetra-(n-butyl)ammonium iodide; triethylamine; acetyl chloride; lithium hexamethyldisilazane; In tetrahydrofuran; N,N-dimethyl-formamide; 2: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1021/jo501302f