Technology Process of β-(3,5-Dimethylphenyl)ethanesulfonyl azide
There total 3 articles about β-(3,5-Dimethylphenyl)ethanesulfonyl azide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium azide;
In
water; acetone;
for 12h;
Ambient temperature;
DOI:10.1021/jo00200a022
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 48 percent / Phosphorous tribromide / 0.17 h / Heating
2: 1) anhydrous sodium sulfite 2) dimethylformamide, thionyl chloride / 1) water, reflux, 24 h 2) benzene, reflux, 4h
3: 70 percent / Sodium azide / acetone; H2O / 12 h / Ambient temperature
With
thionyl chloride; sodium azide; phosphorus tribromide; N,N-dimethyl-formamide; sodium sulfite;
In
water; acetone;
DOI:10.1021/jo00200a022
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1) anhydrous sodium sulfite 2) dimethylformamide, thionyl chloride / 1) water, reflux, 24 h 2) benzene, reflux, 4h
2: 70 percent / Sodium azide / acetone; H2O / 12 h / Ambient temperature
With
thionyl chloride; sodium azide; N,N-dimethyl-formamide; sodium sulfite;
In
water; acetone;
DOI:10.1021/jo00200a022
