(2R)-5-[(4-methoxybenzyl)oxy]-2-{(3S)-3-methyl-2-methylene-4-[(triisopropylsilyl)oxy]butoxy}pentanal

Base Information

Chemical Name:(2R)-5-[(4-methoxybenzyl)oxy]-2-{(3S)-3-methyl-2-methylene-4-[(triisopropylsilyl)oxy]butoxy}pentanal
CAS No.:232280-11-4
Molecular Formula:C₂₈H₄₈O₅Si
Molecular Weight:492.772
Hs Code.:

Synonyms:(2R)-5-[(4-methoxybenzyl)oxy]-2-{(3S)-3-methyl-2-methylene-4-[(triisopropylsilyl)oxy]butoxy}pentanal

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Chemical Property of (2R)-5-[(4-methoxybenzyl)oxy]-2-{(3S)-3-methyl-2-methylene-4-[(triisopropylsilyl)oxy]butoxy}pentanal

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Technology Process of (2R)-5-[(4-methoxybenzyl)oxy]-2-{(3S)-3-methyl-2-methylene-4-[(triisopropylsilyl)oxy]butoxy}pentanal

There total 9 articles about (2R)-5-[(4-methoxybenzyl)oxy]-2-{(3S)-3-methyl-2-methylene-4-[(triisopropylsilyl)oxy]butoxy}pentanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₅₂O₆Si

: 232280-11-4
(2R)-5-[(4-methoxybenzyl)oxy]-2-{(3S)-3-methyl-2-methylene-4-[(triisopropylsilyl)oxy]butoxy}pentanal

Guidance literature:: With sodium periodate; In tetrahydrofuran; water; at 20 ℃; for 1.5h;
DOI:10.1021/jo702111u

Reference yield:

: (2R,3R)-6-(4-Methoxy-benzyloxy)-3-((S)-3-methyl-2-methylene-4-triisopropylsilanyloxy-butoxy)-hexane-1,2-diol

: 232280-11-4
(2R)-5-[(4-methoxybenzyl)oxy]-2-{(3S)-3-methyl-2-methylene-4-[(triisopropylsilyl)oxy]butoxy}pentanal

Guidance literature:: With sodium periodate; water; In tetrahydrofuran; Yield given;

Reference yield:

: 232280-19-2
(2R,3R)-1,2-O-isopropylidene-6-[(4-methoxybenzyl)oxy]-3-{(3S)-3-methyl-2-methylene-4-[(triisopropylsilyl)oxy]butoxy}hexane-1,2-diol

: 232280-11-4
(2R)-5-[(4-methoxybenzyl)oxy]-2-{(3S)-3-methyl-2-methylene-4-[(triisopropylsilyl)oxy]butoxy}pentanal

Guidance literature:: Multi-step reaction with 2 steps

1: PPTS / ethane-1,2-diol; tetrahydrofuran; CH₂Cl₂ / Heating

2: NaIO₄, H₂O / tetrahydrofuran

With sodium periodate; water; pyridinium p-toluenesulfonate; In tetrahydrofuran; dichloromethane; ethylene glycol;