BFCl₂*Et₂O

Base Information

Chemical Name:BFCl₂*Et₂O
CAS No.:99919-69-4
Molecular Formula:C₄H₁₀BCl₂FO
Molecular Weight:174.838
Hs Code.:

Synonyms:BFCl₂*Et₂O

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Chemical Property of BFCl₂*Et₂O

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Technology Process of BFCl₂*Et₂O

There total 1 articles about BFCl₂*Et₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

: 444-40-6
2,4,6-tris(trilfuoromethyl)phenyllithium

: 10294-34-5
boron trichloride

: 99919-68-3
BF₂Cl*Et₂O

: 99919-69-4
BFCl₂*Et₂O

: 109-63-7
boron trifluoride diethyl etherate

: 681812-01-1
2,4,6-(CF₃)3C₆H₂BCl₂

: 681812-02-2
bis-(2,4,6-tris-trifluoromethyl-phenyl) fluoroborane

Guidance literature:: In diethyl ether; under an inert atm.; to a soln. of Li-contg. compd. in hexanes and Et2O was added dropwise an excess of B-contg. compd. (1 M in heptane) at -78°C ; the react. mixt. was allowed to warm to room temp. for 6 h; the soln. was filtered and the solvents were removed under vac.; a mixt.of yellow oil and white solid; the mixt. was vac. distd. at 60°C /0.05 Torr; the residue was sublimed at 95°C under vac.;
DOI:10.1039/b309820f