hepta-O-benzyl-2'-O-(6-deoxy-α-D-xylo-hex-5-enopyranosyl)-β-D-fructopyranoside

Base Information

Chemical Name:hepta-O-benzyl-2'-O-(6-deoxy-α-D-xylo-hex-5-enopyranosyl)-β-D-fructopyranoside
CAS No.:364781-13-5
Molecular Formula:C₆₁H₆₂O₁₀
Molecular Weight:955.157
Hs Code.:

Synonyms:hepta-O-benzyl-2'-O-(6-deoxy-α-D-xylo-hex-5-enopyranosyl)-β-D-fructopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of hepta-O-benzyl-2'-O-(6-deoxy-α-D-xylo-hex-5-enopyranosyl)-β-D-fructopyranoside

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Technology Process of hepta-O-benzyl-2'-O-(6-deoxy-α-D-xylo-hex-5-enopyranosyl)-β-D-fructopyranoside

There total 3 articles about hepta-O-benzyl-2'-O-(6-deoxy-α-D-xylo-hex-5-enopyranosyl)-β-D-fructopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 100-39-0
benzyl bromide

: 364781-15-7
1',2,3,3',4',6'-hexa-O-benzyl-6-deoxy-6-iodo-sucrose

: 364781-13-5
hepta-O-benzyl-2'-O-(6-deoxy-α-D-xylo-hex-5-enopyranosyl)-β-D-fructopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 22h;
DOI:10.1560/DJYX-KN0A-FGNW-TEQM

Reference yield:

: 89499-92-3
2,3-di-O-benzyl-4,6-O-isopropylidene-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

: 364781-13-5
hepta-O-benzyl-2'-O-(6-deoxy-α-D-xylo-hex-5-enopyranosyl)-β-D-fructopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / aq. AcOH / acetone / 0.5 h / 80 °C

2: 93 percent / I₂; Ph₃P; imidazole / toluene / 2.5 h / 70 °C

3: 98 percent / NaH / dimethylformamide / 22 h / 20 °C

With 1H-imidazole; iodine; sodium hydride; acetic acid; triphenylphosphine; In N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1560/DJYX-KN0A-FGNW-TEQM

Reference yield:

: 89499-93-4
2,3-di-O-benzyl-α-D-glucopyranosyl 1,3,4,6-tetra-O-benzyl-β-D-fructofuranoside

: 364781-13-5
hepta-O-benzyl-2'-O-(6-deoxy-α-D-xylo-hex-5-enopyranosyl)-β-D-fructopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / I₂; Ph₃P; imidazole / toluene / 2.5 h / 70 °C

2: 98 percent / NaH / dimethylformamide / 22 h / 20 °C

With 1H-imidazole; iodine; sodium hydride; triphenylphosphine; In N,N-dimethyl-formamide; toluene;
DOI:10.1560/DJYX-KN0A-FGNW-TEQM