((C₆H₅)2PC₆H₄NC₆H₄P(CH(CH₃)2)2)AlH₂

Base Information

Chemical Name:((C₆H₅)2PC₆H₄NC₆H₄P(CH(CH₃)2)2)AlH₂
CAS No.:1158490-06-2
Molecular Formula:C₃₀H₃₄AlNP₂
Molecular Weight:497.536
Hs Code.:

((C<sub>6</sub>H<sub>5</sub>)2PC<sub>6</sub>H<sub>4</sub>NC<sub>6</sub>H<sub>4</sub>P(CH(CH<sub>3</sub>)2)2)AlH<sub>2</sub>

Synonyms:((C₆H₅)2PC₆H₄NC₆H₄P(CH(CH₃)2)2)AlH₂

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Chemical Property of ((C₆H₅)2PC₆H₄NC₆H₄P(CH(CH₃)2)2)AlH₂

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Technology Process of ((C₆H₅)2PC₆H₄NC₆H₄P(CH(CH₃)2)2)AlH₂

There total 2 articles about ((C₆H₅)2PC₆H₄NC₆H₄P(CH(CH₃)2)2)AlH₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 16853-85-3
lithium aluminium tetrahydride

: 7446-70-0
aluminium trichloride

: 1034653-32-1
HN(o-C₆H₄PPh₂)(o-C₆H₄P(iPr)2)

: 1158490-06-2
((C₆H₅)2PC₆H₄NC₆H₄P(CH(CH₃)2)2)AlH₂

Guidance literature:: With n-BuLi; In tetrahydrofuran; under N2; n-BuLi added to THF soln. of ligand at -35°C; stirred at room temp. for 1 h; cooled to -35°C; solid AlCl3 added; stirredat room temp. for 1 h; solid LiAlH4 added at room temp.; stirred at roo m temp. for 1 h; volatiles removed in vac.; extd. with toluene; filtered through Celite; toluene evapd. under reduced pressure; elem. anal.;
DOI:10.1021/ic802030d

Reference yield:

: 16853-85-3
lithium aluminium tetrahydride

: 1034653-32-1
HN(o-C₆H₄PPh₂)(o-C₆H₄P(iPr)2)

: 917-65-7
methylaluminum dichloride

: 1158490-06-2
((C₆H₅)2PC₆H₄NC₆H₄P(CH(CH₃)2)2)AlH₂

Guidance literature:: In toluene; under N2; MeAlCl2 added to ligand in toluene at -35°C; LiAlH4 added at room temp.; stirred at room temp. for 1 h; volatiles removed in vac.; extd. with toluene; filtered through Celite; toluene evapd. under reduced pressure; elem. anal.;
DOI:10.1021/ic802030d