N,N-diethyl-N'-pentafluorophenylacetamidine

Base Information

• Chemical Name: N,N-diethyl-N'-pentafluorophenylacetamidine
• CAS No.: 141249-68-5
• Molecular Formula: C₁₂H₁₃F₅N₂
• Molecular Weight: 280.241
• Mol file: 141249-68-5.mol

Synonyms:N,N-diethyl-N'-pentafluorophenylacetamidine

Chemical Property of N,N-diethyl-N'-pentafluorophenylacetamidine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N-diethyl-N'-pentafluorophenylacetamidine

There total 2 articles about N,N-diethyl-N'-pentafluorophenylacetamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

perfluorophenyl azide (1423-15-0) + diethylamine (109-89-7) → N,N-diethyl-N'-pentafluorophenylformamide (141249-67-4) + 1,1-diethyl-2-pentafluorophenylhydrazine (123228-10-4) + N,N-diethyl-N'-pentafluorophenylacetamidine (141249-68-5)

Guidance literature:

Irradiation;

DOI:10.1016/S0040-4039(00)99647-3

Reference yield:

pentafluorophenyl hydrazine (828-73-9) → N,N-diethyl-N'-pentafluorophenylacetamidine (141249-68-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 33 percent / aq. HCl, NaNO₂ / diethyl ether / 1 h / 0 °C

2: 1.5 percent / 24 h / Ambient temperature; Irradiation

With hydrogenchloride; sodium nitrite; In diethyl ether;

DOI:10.1021/ja00039a016

upstream raw materials:

perfluorophenyl azide

diethylamine

pentafluorophenyl hydrazine