tert-butyl 2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-(E)-cyclohexylidene-1-acetate

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Chemical Name:tert-butyl 2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-(E)-cyclohexylidene-1-acetate
CAS No.:171051-36-8
Molecular Formula:C₂₉H₃₀N₄O₃
Molecular Weight:482.582
Hs Code.:

Synonyms:tert-butyl 2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-(E)-cyclohexylidene-1-acetate

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Chemical Property of tert-butyl 2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-(E)-cyclohexylidene-1-acetate

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Technology Process of tert-butyl 2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-(E)-cyclohexylidene-1-acetate

There total 8 articles about tert-butyl 2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-(E)-cyclohexylidene-1-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 27784-76-5
tert-butyl diethylphosphonoacetate

: 171050-40-1
3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-(6H)-pyridazin-6-one-1-cyclohexan-2-one

: 171051-36-8
tert-butyl 2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-(E)-cyclohexylidene-1-acetate

: 171051-35-7
tert-butyl 6-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-1-cyclohexenylacetate

: 171051-34-6
tert-butyl 2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-1-cyclohexenylacetate

Guidance literature:: tert-butyl diethylphosphonoacetate; With sodium hydride; In toluene; at 4 ℃; for 0.5h;

3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-(6H)-pyridazin-6-one-1-cyclohexan-2-one; In toluene; at 24 ℃; for 24h;
DOI:10.1016/S0040-4020(99)00590-6

Reference yield: 49.0%

: 27784-76-5
tert-butyl diethylphosphonoacetate

: 171050-40-1
3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-(6H)-pyridazin-6-one-1-cyclohexan-2-one

: 171051-40-4
tert-butyl 2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-(Z)-cyclohexylidene-1-acetate

: 171051-36-8
tert-butyl 2-[6-oxo-3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-1(6H)-pyridazinyl]-(E)-cyclohexylidene-1-acetate

Guidance literature:: tert-butyl diethylphosphonoacetate; With 18-crown-6 ether; potassium tert-butylate; In toluene; at 4 ℃; for 0.5h;

3-(2-phenylpyrazolo[1,5-a]pyridin-3-yl)-(6H)-pyridazin-6-one-1-cyclohexan-2-one; In toluene; at 20 ℃; for 8h;
DOI:10.1016/S0040-4020(99)00590-6