(2S,5R)-2-isopropyl-5-methyl cyclohexyl-2-azidoacetate

Base Information

Chemical Name:(2S,5R)-2-isopropyl-5-methyl cyclohexyl-2-azidoacetate
CAS No.:130156-93-3
Molecular Formula:C₁₂H₂₁N₃O₂
Molecular Weight:239.318
Hs Code.:

Synonyms:(2S,5R)-2-isopropyl-5-methyl cyclohexyl-2-azidoacetate

Suppliers and Price of (2S,5R)-2-isopropyl-5-methyl cyclohexyl-2-azidoacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,5R)-2-isopropyl-5-methyl cyclohexyl-2-azidoacetate

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Technology Process of (2S,5R)-2-isopropyl-5-methyl cyclohexyl-2-azidoacetate

There total 2 articles about (2S,5R)-2-isopropyl-5-methyl cyclohexyl-2-azidoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 7377-98-2,27994-88-3,88644-14-8,106916-72-7,111957-92-7,21758-29-2
(-)-menthyl chloroacetate

: 130156-93-3
(2S,5R)-2-isopropyl-5-methyl cyclohexyl-2-azidoacetate

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; for 4h; Inert atmosphere; Heating;
DOI:10.1002/jhet.4286

Reference yield:

: 2216-51-5
(-)-menthol

: 130156-93-3
(2S,5R)-2-isopropyl-5-methyl cyclohexyl-2-azidoacetate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 1.33 h / 0 - 20 °C / Inert atmosphere

2: sodium azide / N,N-dimethyl-formamide / 4 h / Inert atmosphere; Heating

With pyridine; sodium azide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/jhet.4286