2-ACETAMIDO-2-DEOXY-B-D-GLUCOSYLAMINE

Base Information

• Chemical Name: 2-ACETAMIDO-2-DEOXY-B-D-GLUCOSYLAMINE
• CAS No.: 18615-50-4
• Molecular Formula: C8H16 N2 O5
• Molecular Weight: 220.225
• Hs Code.: 2932999099
• Mol file: 18615-50-4.mol

Synonyms:2-ACETAMIDO-2-DEOXY-BETA-D-GLUCOSYLAMINE;2-ACETAMIDO-2-DEOXY-BETA-D-GLUCOPYRANOSYL AMINE;2-ACETAMIDO-2-DEOXY-B-D-GLUCOSYLAMINE;2-ACETAMIDO-2-DEOXY-B-D-GLUCOPYRANOSYLAMIN , 95% MIN.;N-Acetyl-b-glucosaminylamine;2-Acetamido-2-deoxy-β-D-glucopyranosylamine

Chemical Property of 2-ACETAMIDO-2-DEOXY-B-D-GLUCOSYLAMINE

Chemical Property:

• Melting Point: 103-112°C
• PSA: 125.04000
• LogP: -2.02000
• Storage Temp.: −20°C

Purity/Quality:

98%min ^*data from raw suppliers

2-Acetamido-2-deoxy-b-D-glucosylamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-ACETAMIDO-2-DEOXY-B-D-GLUCOSYLAMINE

There total 4 articles about 2-ACETAMIDO-2-DEOXY-B-D-GLUCOSYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

1-N-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosylamine (6205-72-7) → 1-N-acetyl-2-amino-2-deoxy-β-D-glucopyranosylamine (18615-50-4)

Guidance literature:

With hydrazine; at 100 ℃; for 30h;

DOI:10.1016/0008-6215(83)88252-4

Reference yield:

1-N-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosylamine (6205-72-7) → 3,5-dimethyl-4H-1,2,4-triazol-4-amine (3530-15-2) + 1-N-acetyl-2-amino-2-deoxy-β-D-glucopyranosylamine (18615-50-4) + acetic acid hydrazide (1068-57-1) + 2-amino-2-deoxy-D-glucose hydrazone (77045-60-4,131158-04-8)

Guidance literature:

With hydrazine; at 100 ℃; for 30h; Product distribution; other temp., time and cat.;

DOI:10.1016/0008-6215(83)84008-7

Reference yield:

(+)-D-glucosamine hydrochloride (1078691-95-8) + acetic acid hydrazide (1068-57-1) → 1-N-acetyl-2-amino-2-deoxy-β-D-glucopyranosylamine (18615-50-4)

Guidance literature:

In water-d2; for 16h; Ambient temperature;

DOI:10.1016/S0008-6215(00)85432-4

upstream raw materials:

1-N-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosylamine

(+)-D-glucosamine hydrochloride

acetic acid hydrazide