1-[2-(4,4-dimethyl(1,3-oxazolin-2-yl))-4-methoxyphenyl]-5-methoxyindan-1-ol

Base Information

Chemical Name:1-[2-(4,4-dimethyl(1,3-oxazolin-2-yl))-4-methoxyphenyl]-5-methoxyindan-1-ol
CAS No.:678996-41-3
Molecular Formula:C₂₂H₂₅NO₄
Molecular Weight:367.445
Hs Code.:

Synonyms:1-[2-(4,4-dimethyl(1,3-oxazolin-2-yl))-4-methoxyphenyl]-5-methoxyindan-1-ol

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Chemical Property of 1-[2-(4,4-dimethyl(1,3-oxazolin-2-yl))-4-methoxyphenyl]-5-methoxyindan-1-ol

Chemical Property:

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Technology Process of 1-[2-(4,4-dimethyl(1,3-oxazolin-2-yl))-4-methoxyphenyl]-5-methoxyindan-1-ol

There total 1 articles about 1-[2-(4,4-dimethyl(1,3-oxazolin-2-yl))-4-methoxyphenyl]-5-methoxyindan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5111-70-6
5-methoxy-1-indanone

: C₁₂H₁₄BrMgNO₂

: 678996-41-3
1-[2-(4,4-dimethyl(1,3-oxazolin-2-yl))-4-methoxyphenyl]-5-methoxyindan-1-ol

Guidance literature:: In tetrahydrofuran; at 20 ℃;
DOI:10.1021/jm034134+

Reference yield:

: 678996-41-3
1-[2-(4,4-dimethyl(1,3-oxazolin-2-yl))-4-methoxyphenyl]-5-methoxyindan-1-ol

: 609337-91-9
5-methoxy-2-(5-methoxy-1-indanyl)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: aq. H₂SO₄ / dioxane / 6 h / Heating

2: 135 g / H₂; AcOH / Pd(OH)2/C / 12 h / 20 °C / 760 Torr

With sulfuric acid; hydrogen; acetic acid; palladium dihydroxide; In 1,4-dioxane;
DOI:10.1021/jm034134+

Reference yield:

: 678996-41-3
1-[2-(4,4-dimethyl(1,3-oxazolin-2-yl))-4-methoxyphenyl]-5-methoxyindan-1-ol

: 678996-42-4
5-methoxy-2-(5-methoxy-indan-1-yl)-benzoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: aq. H₂SO₄ / dioxane / 6 h / Heating

2: 135 g / H₂; AcOH / Pd(OH)2/C / 12 h / 20 °C / 760 Torr

3: (COCl)2; DMF / toluene / 4 h / 20 °C

With oxalyl dichloride; sulfuric acid; hydrogen; acetic acid; N,N-dimethyl-formamide; palladium dihydroxide; In 1,4-dioxane; toluene;
DOI:10.1021/jm034134+