N₁-[4-(phenylsulfonyl)benzoyl]-N₄-(3,4,5-trimethoxyphenyl)-thiosemicarbazide

Base Information

Chemical Name:N₁-[4-(phenylsulfonyl)benzoyl]-N₄-(3,4,5-trimethoxyphenyl)-thiosemicarbazide
CAS No.:1361970-44-6
Molecular Formula:C₂₃H₂₃N₃O₆S₂
Molecular Weight:501.584
Hs Code.:

N<sub>1</sub>-[4-(phenylsulfonyl)benzoyl]-N<sub>4</sub>-(3,4,5-trimethoxyphenyl)-thiosemicarbazide

Synonyms:N₁-[4-(phenylsulfonyl)benzoyl]-N₄-(3,4,5-trimethoxyphenyl)-thiosemicarbazide

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Chemical Property of N₁-[4-(phenylsulfonyl)benzoyl]-N₄-(3,4,5-trimethoxyphenyl)-thiosemicarbazide

Chemical Property:

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Technology Process of N₁-[4-(phenylsulfonyl)benzoyl]-N₄-(3,4,5-trimethoxyphenyl)-thiosemicarbazide

There total 6 articles about N₁-[4-(phenylsulfonyl)benzoyl]-N₄-(3,4,5-trimethoxyphenyl)-thiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.2%

: 35967-24-9
(3,4,5-trimethoxyphenyl)isothiocyanate

: 20721-07-7
p-(Phenylsulphonyl) benzoic acid hydrazide

: 1361970-44-6
N₁-[4-(phenylsulfonyl)benzoyl]-N₄-(3,4,5-trimethoxyphenyl)-thiosemicarbazide

Guidance literature:: In ethanol; Reflux;
DOI:10.1016/j.ejmech.2012.01.031

Reference yield:

: 640-57-3
phenyltolylsulfone

: 1361970-44-6
N₁-[4-(phenylsulfonyl)benzoyl]-N₄-(3,4,5-trimethoxyphenyl)-thiosemicarbazide

Guidance literature:: Multi-step reaction with 4 steps

1: chromium(VI) oxide; acetic acid

2: sulfuric acid

3: hydrazine hydrate

4: ethanol / Reflux

With chromium(VI) oxide; sulfuric acid; hydrazine hydrate; acetic acid; In ethanol;
DOI:10.1016/j.ejmech.2012.01.031

Reference yield:

: 5361-54-6
4-(phenylsulfonyl)benzoic acid

: 1361970-44-6
N₁-[4-(phenylsulfonyl)benzoyl]-N₄-(3,4,5-trimethoxyphenyl)-thiosemicarbazide

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid

2: hydrazine hydrate

3: ethanol / Reflux

With sulfuric acid; hydrazine hydrate; In ethanol;
DOI:10.1016/j.ejmech.2012.01.031