[16-(2,3-Bis-benzyloxy-benzoyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl]-(2,3-bis-benzyloxy-phenyl)-methanone

Base Information

Chemical Name:[16-(2,3-Bis-benzyloxy-benzoyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl]-(2,3-bis-benzyloxy-phenyl)-methanone
CAS No.:160358-51-0
Molecular Formula:C₅₄H₅₈N₂O₁₀
Molecular Weight:895.062
Hs Code.:

Synonyms:[16-(2,3-Bis-benzyloxy-benzoyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl]-(2,3-bis-benzyloxy-phenyl)-methanone

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Chemical Property of [16-(2,3-Bis-benzyloxy-benzoyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl]-(2,3-bis-benzyloxy-phenyl)-methanone

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Technology Process of [16-(2,3-Bis-benzyloxy-benzoyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl]-(2,3-bis-benzyloxy-phenyl)-methanone

There total 5 articles about [16-(2,3-Bis-benzyloxy-benzoyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl]-(2,3-bis-benzyloxy-phenyl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 69146-58-3
2,3-bis(benzyloxy)benzoyl chloride

: 23978-55-4
1,4,10,13-tetraoxa-7,16-diazacyclooctadecane

: 160358-51-0
[16-(2,3-Bis-benzyloxy-benzoyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl]-(2,3-bis-benzyloxy-phenyl)-methanone

Guidance literature:: With triethylamine; In toluene; for 2.25h; Ambient temperature;
DOI:10.1016/0040-4039(94)80116-9

Reference yield:

: 5779-91-9
2,3-bis(benzyloxy)benzaldehyde

: 160358-51-0
[16-(2,3-Bis-benzyloxy-benzoyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl]-(2,3-bis-benzyloxy-phenyl)-methanone

Guidance literature:: Multi-step reaction with 3 steps

1: NaClO₂, H₂NSO₃H / acetone; H₂O / Ambient temperature

2: SOCl₂ / dimethylformamide

3: 97 percent / Et₃N / toluene / 2.25 h / Ambient temperature

With sodium chlorite; thionyl chloride; aminosulfonic acid; triethylamine; In water; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/0040-4039(94)80116-9

Reference yield:

: 24677-78-9
2,3-dihydroxybenzaldehyde

: 160358-51-0
[16-(2,3-Bis-benzyloxy-benzoyl)-1,4,10,13-tetraoxa-7,16-diaza-cyclooctadec-7-yl]-(2,3-bis-benzyloxy-phenyl)-methanone

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃ / ethanol

2: NaClO₂, H₂NSO₃H / acetone; H₂O / Ambient temperature

3: SOCl₂ / dimethylformamide

4: 97 percent / Et₃N / toluene / 2.25 h / Ambient temperature

With sodium chlorite; thionyl chloride; aminosulfonic acid; potassium carbonate; triethylamine; In ethanol; water; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/0040-4039(94)80116-9