Methyl-3-(9-benzyl-2-methyl-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)propionat

Base Information

Chemical Name:Methyl-3-(9-benzyl-2-methyl-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)propionat
CAS No.:143076-84-0
Molecular Formula:C₂₃H₂₆N₂O₂
Molecular Weight:362.472
Hs Code.:

Synonyms:Methyl-3-(9-benzyl-2-methyl-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)propionat

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Chemical Property of Methyl-3-(9-benzyl-2-methyl-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)propionat

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Technology Process of Methyl-3-(9-benzyl-2-methyl-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)propionat

There total 4 articles about Methyl-3-(9-benzyl-2-methyl-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)propionat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 67-56-1
methanol

: 143076-83-9
3-(9-Benzyl-2-methyl-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)propionsaeure

: 143076-84-0
Methyl-3-(9-benzyl-2-methyl-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)propionat

Guidance literature:: With sulfuric acid; for 5h; Heating;

Reference yield:

: 65284-87-9
3-methyl-1,2,3,3a,4,5-hexahydro-indolo[3,2,1-de][1,5]naphthyridin-6-one

: 143076-84-0
Methyl-3-(9-benzyl-2-methyl-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)propionat

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / 15percent aq. KOH / ethanol / 2 h / Heating

2: 1) NaH / 1) DMSO, r. t., 1h , 2) DMSO, r. t.

3: 78 percent / conc. H₂SO₄ / 5 h / Heating

With potassium hydroxide; sulfuric acid; sodium hydride; In ethanol;

Reference yield:

: 100-39-0
benzyl bromide

: 143076-84-0
Methyl-3-(9-benzyl-2-methyl-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-yl)propionat

Guidance literature:: Multi-step reaction with 2 steps

1: 1) NaH / 1) DMSO, r. t., 1h , 2) DMSO, r. t.

2: 78 percent / conc. H₂SO₄ / 5 h / Heating

With sulfuric acid; sodium hydride;