C₁₅H₁₉ClN₂O₄*ClH

Base Information

Chemical Name:C₁₅H₁₉ClN₂O₄*ClH
CAS No.:889857-34-5
Molecular Formula:C₁₅H₁₉ClN₂O₄*ClH
Molecular Weight:363.241
Hs Code.:

C<sub>15</sub>H<sub>19</sub>ClN<sub>2</sub>O<sub>4</sub>*ClH

Synonyms:C₁₅H₁₉ClN₂O₄*ClH

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Chemical Property of C₁₅H₁₉ClN₂O₄*ClH

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Technology Process of C₁₅H₁₉ClN₂O₄*ClH

There total 8 articles about C₁₅H₁₉ClN₂O₄*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₂₇ClN₂O₆

: 889857-34-5
C₁₅H₁₉ClN₂O₄*ClH

Guidance literature:: With hydrogenchloride; In ethyl acetate; at 20 ℃; for 0.333333h;
DOI:10.1016/j.bmc.2013.04.079

Reference yield:

: 7035-09-8
5-chloro-2-methoxybenzaldehyde

: 889857-34-5
C₁₅H₁₉ClN₂O₄*ClH

Guidance literature:: Multi-step reaction with 8 steps

1: 1,4-diaza-bicyclo[2.2.2]octane; lanthanum(lll) triflate; 2,2'-iminobis[ethanol] / 60 h / 20 °C

2: triethylamine; pyridine / dichloromethane / 1 h / 0 °C

3: sodium azide / dimethyl sulfoxide / 0.5 h / 20 °C

4: triphenylphosphine / tetrahydrofuran; water / 15 h / 20 °C

5: sodium hydroxide; water / methanol / 2 h / 20 °C

6: sodium hydroxide; water / tetrahydrofuran / 1 h / 20 °C

7: triethylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C / Cooling with ice

8: hydrogenchloride / ethyl acetate / 0.33 h / 20 °C

With pyridine; 1,4-diaza-bicyclo[2.2.2]octane; hydrogenchloride; sodium azide; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; 2,2'-iminobis[ethanol]; triphenylphosphine; sodium hydroxide; lanthanum(lll) triflate; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; 1: |Baylis-Hillman Reaction;
DOI:10.1016/j.bmc.2013.04.079

Reference yield:

: 889855-37-2
methyl 2-[(5-chloro-2-methoxyphenyl)(hydroxy)methyl]propenoate

: 889857-34-5
C₁₅H₁₉ClN₂O₄*ClH

Guidance literature:: Multi-step reaction with 7 steps

1: triethylamine; pyridine / dichloromethane / 1 h / 0 °C

2: sodium azide / dimethyl sulfoxide / 0.5 h / 20 °C

3: triphenylphosphine / tetrahydrofuran; water / 15 h / 20 °C

4: sodium hydroxide; water / methanol / 2 h / 20 °C

5: sodium hydroxide; water / tetrahydrofuran / 1 h / 20 °C

6: triethylamine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C / Cooling with ice

7: hydrogenchloride / ethyl acetate / 0.33 h / 20 °C

With pyridine; hydrogenchloride; sodium azide; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate;
DOI:10.1016/j.bmc.2013.04.079