C₂₅H₂₂INO₂S

Base Information

Chemical Name:C₂₅H₂₂INO₂S
CAS No.:1585185-84-7
Molecular Formula:C₂₅H₂₂INO₂S
Molecular Weight:527.426
Hs Code.:

C<sub>25</sub>H<sub>22</sub>INO<sub>2</sub>S

Synonyms:C₂₅H₂₂INO₂S

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Chemical Property of C₂₅H₂₂INO₂S

Chemical Property:

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Technology Process of C₂₅H₂₂INO₂S

There total 5 articles about C₂₅H₂₂INO₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1585185-91-6
C₂₅H₂₂INO₂S

: 1585185-84-7
C₂₅H₂₂INO₂S

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1016/j.tetlet.2014.02.087

Reference yield:

: 1504-58-1
3-Phenyl-2-propyn-1-ol

: 1585185-84-7
C₂₅H₂₂INO₂S

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper(l) iodide / diethyl ether / 18 h / -78 - 20 °C / Inert atmosphere

1.2: 3 h / -78 - 20 °C / Inert atmosphere

2.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 20 °C

3.1: potassium carbonate; sodium iodide / 20 - 80 °C

4.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C

With copper(l) iodide; di-isopropyl azodicarboxylate; potassium tert-butylate; potassium carbonate; triphenylphosphine; sodium iodide; In tetrahydrofuran; diethyl ether; 2.1: |Mitsunobu Displacement;
DOI:10.1016/j.tetlet.2014.02.087

Reference yield:

: 1350810-15-9
C₂₂H₂₀INO₂S

: 1585185-84-7
C₂₅H₂₂INO₂S

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; sodium iodide / 20 - 80 °C

2: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C

With potassium tert-butylate; potassium carbonate; sodium iodide; In tetrahydrofuran;
DOI:10.1016/j.tetlet.2014.02.087