Fmoc-phenylalanine ketoacid

Base Information

Chemical Name:Fmoc-phenylalanine ketoacid
CAS No.:1137148-17-4
Molecular Formula:C₂₅H₂₁NO₅
Molecular Weight:415.445
Hs Code.:

Synonyms:Fmoc-phenylalanine ketoacid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Fmoc-phenylalanine ketoacid

Chemical Property:

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Technology Process of Fmoc-phenylalanine ketoacid

There total 2 articles about Fmoc-phenylalanine ketoacid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₀H₂₈N₂O₃S

: 1137148-17-4
Fmoc-phenylalanine ketoacid

Guidance literature:: With Oxone; In water; N,N-dimethyl-formamide; at 20 ℃; for 0.5h;
DOI:10.1016/j.bmc.2015.07.023

Reference yield:

: 35661-40-6
N-Fmoc L-Phe

: 1137148-17-4
Fmoc-phenylalanine ketoacid

Guidance literature:: Multi-step reaction with 2 steps

1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 14 h / 0 - 20 °C

2: Oxone / N,N-dimethyl-formamide; water / 0.5 h / 20 °C

With Oxone; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2015.07.023

Reference yield: 97.0%

: 1137148-17-4
Fmoc-phenylalanine ketoacid

: 149-73-5
trimethyl orthoformate

: C₂₇H₂₇NO₆

Guidance literature:: With sulfuric acid; In neat (no solvent); at 20 ℃; for 15h; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.orglett.6b01692