Technology Process of C33H46N6O6
There total 10 articles about C33H46N6O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
ethyl 3-(3-((((3aR,4R,6R,6aS)-6-(6-((2,4-dimethoxybenzyl)amino)-9H-purin-9-yl)-2,2-dimethyltetrahydro-3aH-cyclopenta[d][1,3]dioxol-4-yl)methyl)(isopropyl)amino)cyclobutyl)propanoate;
With
methanol; lithium hydroxide monohydrate;
In
tetrahydrofuran;
at 20 ℃;
With
hydrogenchloride;
In
tetrahydrofuran; water;
pH=6;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: di-isopropyl azodicarboxylate / tetrahydrofuran / 0.25 h / 0 °C
1.2: 18.5 h
2.1: N-ethyl-N,N-diisopropylamine / butan-1-ol / 16.5 h / 80 °C
3.1: trimethylphosphane / tetrahydrofuran / 2 h / 0 °C
3.2: 2.75 h / 20 °C
4.1: sodium tris(acetoxy)borohydride; methanol / acetic acid / 1,2-dichloro-ethane / 20 °C
5.1: triethylamine / acetonitrile / 20 h / 80 °C
6.1: methanol; lithium hydroxide monohydrate / tetrahydrofuran / 20 °C
6.2: pH 6
With
methanol; lithium hydroxide monohydrate; di-isopropyl azodicarboxylate; sodium tris(acetoxy)borohydride; triethylamine; N-ethyl-N,N-diisopropylamine; trimethylphosphane;
acetic acid;
In
tetrahydrofuran; 1,2-dichloro-ethane; acetonitrile; butan-1-ol;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: zinc/copper couple / diethyl ether / 72 h / 20 °C
2.1: zinc; ammonium chloride / methanol / 3 h / Reflux
3.1: sodium tris(acetoxy)borohydride; methanol / acetic acid / 1,2-dichloro-ethane / 20 °C
4.1: triethylamine / acetonitrile / 20 h / 80 °C
5.1: methanol; lithium hydroxide monohydrate / tetrahydrofuran / 20 °C
5.2: pH 6
With
methanol; lithium hydroxide monohydrate; zinc/copper couple; sodium tris(acetoxy)borohydride; ammonium chloride; triethylamine; zinc;
acetic acid;
In
tetrahydrofuran; methanol; diethyl ether; 1,2-dichloro-ethane; acetonitrile;