(R)-3-(1-Benzyloxy-4-tert-butyldiphenylsilyloxybutan-2-yl)-oxazolidine-2,4-dione

Base Information

Chemical Name:(R)-3-(1-Benzyloxy-4-tert-butyldiphenylsilyloxybutan-2-yl)-oxazolidine-2,4-dione
CAS No.:159142-18-4
Molecular Formula:C₃₀H₃₅NO₅Si
Molecular Weight:517.697
Hs Code.:

Synonyms:(R)-3-(1-Benzyloxy-4-tert-butyldiphenylsilyloxybutan-2-yl)-oxazolidine-2,4-dione

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Chemical Property of (R)-3-(1-Benzyloxy-4-tert-butyldiphenylsilyloxybutan-2-yl)-oxazolidine-2,4-dione

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Technology Process of (R)-3-(1-Benzyloxy-4-tert-butyldiphenylsilyloxybutan-2-yl)-oxazolidine-2,4-dione

There total 6 articles about (R)-3-(1-Benzyloxy-4-tert-butyldiphenylsilyloxybutan-2-yl)-oxazolidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.8%

: 2346-26-1
2,4-oxazolidinedione

: 159142-17-3
(S)-1-Benzyloxy-4-tert-butyldiphenylsilyloxybutan-2-ol

: 159142-18-4
(R)-3-(1-Benzyloxy-4-tert-butyldiphenylsilyloxybutan-2-yl)-oxazolidine-2,4-dione

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; for 12h; Ambient temperature;
DOI:10.1039/P19960000793

Reference yield:

: 116996-52-2
(2S)-4-O-(tert-butyldiphenylsilyl)butane-1,2,4-triol

: 159142-18-4
(R)-3-(1-Benzyloxy-4-tert-butyldiphenylsilyloxybutan-2-yl)-oxazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Bu₂SnO, 2.) Bu₄NBr / 1.) toluene, reflux, 4 h, 2.) 80 deg C, 24 h

2: 64.8 percent / diisopropyl azodicarboxylate, Ph₃P / tetrahydrofuran / 12 h / Ambient temperature

With di-isopropyl azodicarboxylate; tetrabutylammomium bromide; di(n-butyl)tin oxide; triphenylphosphine; In tetrahydrofuran;
DOI:10.1039/P19960000793

Reference yield:

: 146028-83-3
(2S)-1,2-O-isopropylidene-4-(tert-butyldiphenylsilyl)butane-1,2,4-triol

: 159142-18-4
(R)-3-(1-Benzyloxy-4-tert-butyldiphenylsilyloxybutan-2-yl)-oxazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 3 steps

1: p-TsOH*H₂O / methanol / 0.5 h / Ambient temperature

2: 1.) Bu₂SnO, 2.) Bu₄NBr / 1.) toluene, reflux, 4 h, 2.) 80 deg C, 24 h

3: 64.8 percent / diisopropyl azodicarboxylate, Ph₃P / tetrahydrofuran / 12 h / Ambient temperature

With di-isopropyl azodicarboxylate; tetrabutylammomium bromide; di(n-butyl)tin oxide; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; methanol;
DOI:10.1039/P19960000793