1,1-Dibromo-3-cyclohexyl-1-propene

Base Information

Chemical Name:1,1-Dibromo-3-cyclohexyl-1-propene
CAS No.:129765-71-5
Molecular Formula:C₉H₁₄Br₂
Molecular Weight:282.018
Hs Code.:
DSSTox Substance ID:DTXSID801283544

Synonyms:SCHEMBL7269756;BERTUQCHCIUZMG-UHFFFAOYSA-N;DTXSID801283544;1,1-Dibromo-3-cyclohexyl-1-propene;(3,3-Dibromo-2-propen-1-yl)cyclohexane;129765-71-5

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1-Dibromo-3-cyclohexyl-1-propene

Chemical Property:

XLogP3:5.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:281.94418
Heavy Atom Count:11
Complexity:131

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CCC(CC1)CC=C(Br)Br

Technology Process of 1,1-Dibromo-3-cyclohexyl-1-propene

There total 2 articles about 1,1-Dibromo-3-cyclohexyl-1-propene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 558-13-4
carbon tetrabromide

: 5664-21-1
cyclohexylacetaldehyde

: 129765-71-5
3-cyclohexyl-1,1-dibromo-1-propene

Guidance literature:: With triphenylphosphine; Yield given. Multistep reaction; 1) CH₂Cl₂, less than 50 deg C, 5 min, 2) r.t., 30 min;

Reference yield:

: 4442-79-9
cyclohexylethan-1-ol

: 129765-71-5
3-cyclohexyl-1,1-dibromo-1-propene

Guidance literature:: Multi-step reaction with 2 steps

1: 2,2,6,6-tetramethylpiperidinyloxy free radical (TEMPO), sodium bromide, sodium bicarbonate/5percent bleach / CH₂Cl₂; H₂O / 0.5 h

2: triphenylphosphine / CH₂Cl₂; H₂O / 0.5 h / below 30 deg C

With sodium hypochlorite; 4-oxo-2,2,6,6-tetramethylpiperidin-oxyl; sodium hydrogencarbonate; triphenylphosphine; sodium bromide; In dichloromethane; water;
DOI:10.1016/S0040-4020(01)80638-4

Reference yield: 97.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 129765-71-5
3-cyclohexyl-1,1-dibromo-1-propene

: 34452-39-6
4-cyclohexyl-1-hydroxy-2-butyne

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; for 0.5h; Ambient temperature; 1.) below 0 deg C, 30 min;
DOI:10.1016/S0040-4020(01)80638-4