(6S,9S,15S)-methyl 15-(2-amino-2-oxoethyl)-6,9-dibenzyl-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate

Base Information

Chemical Name:(6S,9S,15S)-methyl 15-(2-amino-2-oxoethyl)-6,9-dibenzyl-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate
CAS No.:1620161-89-8
Molecular Formula:C₃₀H₃₉N₅O₈
Molecular Weight:597.668
Hs Code.:

Synonyms:(6S,9S,15S)-methyl 15-(2-amino-2-oxoethyl)-6,9-dibenzyl-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate

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Chemical Property of (6S,9S,15S)-methyl 15-(2-amino-2-oxoethyl)-6,9-dibenzyl-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate

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Technology Process of (6S,9S,15S)-methyl 15-(2-amino-2-oxoethyl)-6,9-dibenzyl-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate

There total 2 articles about (6S,9S,15S)-methyl 15-(2-amino-2-oxoethyl)-6,9-dibenzyl-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1620161-82-1
(6S,9S)-S-4-nitrophenyl 6,9-dibenzyl-2,2-dimethyl-4,7,10-trioxo-3-oxa-5,8,11-triazatridecane-13-thioate

: 6384-09-4,108258-31-7,119991-47-8
methyl (S)-2,4-diamino-4-oxobutanoate

: 1620161-89-8
(6S,9S,15S)-methyl 15-(2-amino-2-oxoethyl)-6,9-dibenzyl-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate

Guidance literature:: With sodium hydrogencarbonate; In dimethyl sulfoxide; at 20 ℃; for 25h; Inert atmosphere;
DOI:10.1021/ol501669n

Reference yield:

: 82816-76-0
N-tert-butoxycarbonyl-L-phenylalanine-L-phenylalanine-glycine

: 1620161-89-8
(6S,9S,15S)-methyl 15-(2-amino-2-oxoethyl)-6,9-dibenzyl-2,2-dimethyl-4,7,10,13-tetraoxo-3-oxa-5,8,11,14-tetraazahexadecan-16-oate

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2: sodium hydrogencarbonate / dimethyl sulfoxide / 25 h / 20 °C / Inert atmosphere

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ol501669n