2-(3-CHLOROPROPYL)-1,3-DIOXOLANE

Base Information

Chemical Name:2-(3-CHLOROPROPYL)-1,3-DIOXOLANE
CAS No.:16686-11-6
Molecular Formula:C6H11 Cl O2
Molecular Weight:150.605
Hs Code.:29329990
Mol file:16686-11-6.mol

Synonyms:1-Ethylenedioxy-4-chlorobutane;2-(3-Chloropropyl)-1,3-dioxolane; 3-Chloro-1-(1,3-dioxolan-2-yl)propane

Suppliers and Price of 2-(3-CHLOROPROPYL)-1,3-DIOXOLANE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-(3-Chloropropyl)-1,3-dioxolane
100mg
$ 60.00

TCI Chemical
2-(3-Chloropropyl)-1,3-dioxolane >97.0%(GC)
25g
$ 520.00

TCI Chemical
2-(3-Chloropropyl)-1,3-dioxolane >97.0%(GC)
5g
$ 110.00

SynQuest Laboratories
2-(3-Chloropropyl)-1,3-dioxolane 95%
1 g
$ 152.00

SynQuest Laboratories
2-(3-Chloropropyl)-1,3-dioxolane 95%
5 g
$ 312.00

SynQuest Laboratories
2-(3-Chloropropyl)-1,3-dioxolane 95%
25 g
$ 1088.00

Sigma-Aldrich
2-(3-Chloropropyl)-1,3-dioxolane ≥97.0% (GC)
25 mL
$ 1130.00

Sigma-Aldrich
2-(3-Chloropropyl)-1,3-dioxolane ≥97.0% (GC)
25ml-f
$ 1130.00

Sigma-Aldrich
2-(3-Chloropropyl)-1,3-dioxolane ≥97.0% (GC)
5 mL
$ 227.00

Sigma-Aldrich
2-(3-Chloropropyl)-1,3-dioxolane ≥97.0% (GC)
5ml-f
$ 217.00

Total 41 raw suppliers

Chemical Property of 2-(3-CHLOROPROPYL)-1,3-DIOXOLANE

Chemical Property:

Vapor Pressure:0.482mmHg at 25°C
Melting Point:80℃
Refractive Index:n20/D 1.453
Boiling Point:93-94 °C12 mm Hg(lit.)
Flash Point:79 °C
PSA：18.46000
Density:1.142 g/mL at 20 °C(lit.)
LogP:1.37830

Purity/Quality:

97% ^*data from raw suppliers

2-(3-Chloropropyl)-1,3-dioxolane ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 23-24/25-36-26

MSDS Files:: SDS file from LookChem

Useful:

Uses 2-(3-Chloropropyl)-1,3-dioxolane (2-(3′-chloropropyl)-1,3-dioxolane) is a masked γ-chlorobutyraldehyde and was used for the introduction of 3-(1,3-dioxolan-2-yl)propyl moiety. It was also used in the synthesis of:(±)-histrionicotoxin and (±)-histrionicotoxin 235A using a two-directional strategy4-iodobutyraldehyde, 5-iodovaleraldehyde and 5-iodo-2-petanonecorresponding phosphonate

Technology Process of 2-(3-CHLOROPROPYL)-1,3-DIOXOLANE

There total 2 articles about 2-(3-CHLOROPROPYL)-1,3-DIOXOLANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6139-84-0
4-chlorobutyraldehyde

: 107-21-1
ethylene glycol

: 16686-11-6
2-(3-chloropropyl)-1,3-dioxolane

Guidance literature:: With toluene-4-sulfonic acid; In benzene; Yield given; Heating;
DOI:10.1016/S0040-4020(98)00333-0

Reference yield:

: 16686-11-6
2-(3-chloropropyl)-1,3-dioxolane

Guidance literature:: DOI:10.1021/ja00789a041

Reference yield: 100.0%

: 16686-11-6
2-(3-chloropropyl)-1,3-dioxolane

: 930-68-7
cyclohexenone

: 328537-73-1
1-[3-(2,5-dioxolanyl)propyl]cyclohex-2-en-1-ol

Guidance literature:: 2-(3-chloropropyl)-1,3-dioxolane; With naphthalene; lithium; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

cyclohexenone; In tetrahydrofuran; at -78 - 20 ℃; for 16h; Inert atmosphere;
DOI:10.1039/c5ob02579f