2-(2-isopropoxy-4,5-dimethoxyphenyl)-4-(3,4-methylenedioxyphenyl)-4-oxobutyric acid

Base Information

Chemical Name:2-(2-isopropoxy-4,5-dimethoxyphenyl)-4-(3,4-methylenedioxyphenyl)-4-oxobutyric acid
CAS No.:323197-78-0
Molecular Formula:C₂₂H₂₄O₈
Molecular Weight:416.428
Hs Code.:

Synonyms:2-(2-isopropoxy-4,5-dimethoxyphenyl)-4-(3,4-methylenedioxyphenyl)-4-oxobutyric acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2-isopropoxy-4,5-dimethoxyphenyl)-4-(3,4-methylenedioxyphenyl)-4-oxobutyric acid

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Technology Process of 2-(2-isopropoxy-4,5-dimethoxyphenyl)-4-(3,4-methylenedioxyphenyl)-4-oxobutyric acid

There total 4 articles about 2-(2-isopropoxy-4,5-dimethoxyphenyl)-4-(3,4-methylenedioxyphenyl)-4-oxobutyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 323197-77-9
2-(4,5-dimethoxy-2-isopropoxyphenyl)-4-(3,4-methylenedioxyphenyl)-4-oxobutyronitrile

: 323197-78-0
2-(2-isopropoxy-4,5-dimethoxyphenyl)-4-(3,4-methylenedioxyphenyl)-4-oxobutyric acid

Guidance literature:: With sodium hydroxide; In ethanol; water; at 90 - 96 ℃; for 3.5h;
DOI:10.1021/jo0012849

Reference yield:

: 323197-76-8
4,5-dimethoxy-2-isopropoxy-3',4'-methylenedioxychalcone

: 323197-78-0
2-(2-isopropoxy-4,5-dimethoxyphenyl)-4-(3,4-methylenedioxyphenyl)-4-oxobutyric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / AcOH / H₂O; various solvent(s) / 1.23 h / 115 °C

2: 90 percent / NaOH / ethanol; H₂O / 3.5 h / 90 - 96 °C

With sodium hydroxide; acetic acid; In ethanol; water;
DOI:10.1021/jo0012849

Reference yield:

: 3162-29-6
1-(benzo[d][1,3]dioxol-6-yl)ethanone

: 323197-78-0
2-(2-isopropoxy-4,5-dimethoxyphenyl)-4-(3,4-methylenedioxyphenyl)-4-oxobutyric acid

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / NaOH / ethanol; H₂O / 20 °C

2: 84 percent / AcOH / H₂O; various solvent(s) / 1.23 h / 115 °C

3: 90 percent / NaOH / ethanol; H₂O / 3.5 h / 90 - 96 °C

With sodium hydroxide; acetic acid; In ethanol; water;
DOI:10.1021/jo0012849