8-(tert-butyldiphenylsilanyloxy)-7-(R)-hydroxyoctanoic acid methyl ester

Base Information

Chemical Name:8-(tert-butyldiphenylsilanyloxy)-7-(R)-hydroxyoctanoic acid methyl ester
CAS No.:1057664-56-8
Molecular Formula:C₂₅H₃₆O₄Si
Molecular Weight:428.644
Hs Code.:

Synonyms:8-(tert-butyldiphenylsilanyloxy)-7-(R)-hydroxyoctanoic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-(tert-butyldiphenylsilanyloxy)-7-(R)-hydroxyoctanoic acid methyl ester

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Technology Process of 8-(tert-butyldiphenylsilanyloxy)-7-(R)-hydroxyoctanoic acid methyl ester

There total 1 articles about 8-(tert-butyldiphenylsilanyloxy)-7-(R)-hydroxyoctanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1057664-56-8
8-(tert-butyldiphenylsilanyloxy)-7-(R)-hydroxyoctanoic acid methyl ester

Guidance literature:

Reference yield: 92.0%

: 1057664-56-8
8-(tert-butyldiphenylsilanyloxy)-7-(R)-hydroxyoctanoic acid methyl ester

: 1057664-57-9
(S)-7-azido-8-(tert-butyldiphenylsilanyloxy)octanoic acid methyl ester

Guidance literature:: With diphenyl phosphoryl azide; triphenylphosphine; diethylazodicarboxylate; In toluene; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jm101092u

Reference yield:

: 1057664-56-8
8-(tert-butyldiphenylsilanyloxy)-7-(R)-hydroxyoctanoic acid methyl ester

: 1057664-59-1
C₂₅H₃₇NO₃Si

Guidance literature:: Multi-step reaction with 2 steps

1: diphenyl phosphoryl azide; triphenylphosphine; diethylazodicarboxylate / toluene / 24 h / 0 - 20 °C

2: hydrogen / palladium 10% on activated carbon / methanol / 18 h

With diphenyl phosphoryl azide; hydrogen; triphenylphosphine; diethylazodicarboxylate; palladium 10% on activated carbon; In methanol; toluene;