7-(S)-tert-butoxycarbonylamino-8-(tert-butyldiphenylsilanyloxy)octanoic acid methyl ester

Base Information

Chemical Name:7-(S)-tert-butoxycarbonylamino-8-(tert-butyldiphenylsilanyloxy)octanoic acid methyl ester
CAS No.:1057664-58-0
Molecular Formula:C₃₀H₄₅NO₅Si
Molecular Weight:527.777
Hs Code.:

Synonyms:7-(S)-tert-butoxycarbonylamino-8-(tert-butyldiphenylsilanyloxy)octanoic acid methyl ester

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Chemical Property of 7-(S)-tert-butoxycarbonylamino-8-(tert-butyldiphenylsilanyloxy)octanoic acid methyl ester

Chemical Property:

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Technology Process of 7-(S)-tert-butoxycarbonylamino-8-(tert-butyldiphenylsilanyloxy)octanoic acid methyl ester

There total 3 articles about 7-(S)-tert-butoxycarbonylamino-8-(tert-butyldiphenylsilanyloxy)octanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1057664-59-1
C₂₅H₃₇NO₃Si

: 24424-99-5
di-tert-butyl dicarbonate

: 1057664-58-0
7-(S)-tert-butoxycarbonylamino-8-(tert-butyldiphenylsilanyloxy)octanoic acid methyl ester

Guidance literature:: In dichloromethane; for 24h;

Reference yield:

: 1057664-56-8
8-(tert-butyldiphenylsilanyloxy)-7-(R)-hydroxyoctanoic acid methyl ester

: 1057664-58-0
7-(S)-tert-butoxycarbonylamino-8-(tert-butyldiphenylsilanyloxy)octanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: diphenyl phosphoryl azide; triphenylphosphine; diethylazodicarboxylate / toluene / 24 h / 0 - 20 °C

2: hydrogen / palladium 10% on activated carbon / methanol / 18 h

3: dichloromethane / 24 h

With diphenyl phosphoryl azide; hydrogen; triphenylphosphine; diethylazodicarboxylate; palladium 10% on activated carbon; In methanol; dichloromethane; toluene;

Reference yield:

: 1057664-57-9
(S)-7-azido-8-(tert-butyldiphenylsilanyloxy)octanoic acid methyl ester

: 1057664-58-0
7-(S)-tert-butoxycarbonylamino-8-(tert-butyldiphenylsilanyloxy)octanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / methanol / 18 h

2: dichloromethane / 24 h

With hydrogen; palladium 10% on activated carbon; In methanol; dichloromethane;