(S)-7-azido-8-(tert-butyldiphenylsilanyloxy)octanoic acid methyl ester

Base Information

Chemical Name:(S)-7-azido-8-(tert-butyldiphenylsilanyloxy)octanoic acid methyl ester
CAS No.:1057664-57-9
Molecular Formula:C₂₅H₃₅N₃O₃Si
Molecular Weight:453.657
Hs Code.:

Synonyms:(S)-7-azido-8-(tert-butyldiphenylsilanyloxy)octanoic acid methyl ester

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Chemical Property of (S)-7-azido-8-(tert-butyldiphenylsilanyloxy)octanoic acid methyl ester

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Technology Process of (S)-7-azido-8-(tert-butyldiphenylsilanyloxy)octanoic acid methyl ester

There total 1 articles about (S)-7-azido-8-(tert-butyldiphenylsilanyloxy)octanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1057664-56-8
8-(tert-butyldiphenylsilanyloxy)-7-(R)-hydroxyoctanoic acid methyl ester

: 1057664-57-9
(S)-7-azido-8-(tert-butyldiphenylsilanyloxy)octanoic acid methyl ester

Guidance literature:: With diphenyl phosphoryl azide; triphenylphosphine; diethylazodicarboxylate; In toluene; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jm101092u

Reference yield: 99.0%

: 1057664-57-9
(S)-7-azido-8-(tert-butyldiphenylsilanyloxy)octanoic acid methyl ester

: 1057664-59-1
C₂₅H₃₇NO₃Si

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In methanol; for 18h;

Reference yield:

: 1057664-57-9
(S)-7-azido-8-(tert-butyldiphenylsilanyloxy)octanoic acid methyl ester

: 1057664-58-0
7-(S)-tert-butoxycarbonylamino-8-(tert-butyldiphenylsilanyloxy)octanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / methanol / 18 h

2: dichloromethane / 24 h

With hydrogen; palladium 10% on activated carbon; In methanol; dichloromethane;