ethyl 2-acetyl-3,5-diiodobenzoate

Base Information

Chemical Name:ethyl 2-acetyl-3,5-diiodobenzoate
CAS No.:524931-72-4
Molecular Formula:C₁₁H₁₀I₂O₃
Molecular Weight:444.008
Hs Code.:

Synonyms:ethyl 2-acetyl-3,5-diiodobenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 2-acetyl-3,5-diiodobenzoate

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Technology Process of ethyl 2-acetyl-3,5-diiodobenzoate

There total 3 articles about ethyl 2-acetyl-3,5-diiodobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 506-96-7
Acetyl bromide

: 25546-12-7
2,3,5-triiodobenzoic acid ethyl ester

: 524931-72-4
ethyl 2-acetyl-3,5-diiodobenzoate

Guidance literature:: 2,3,5-triiodobenzoic acid ethyl ester; With lithium dineopentylcuprate; In diethyl ether; at -78 ℃; for 0.333333h;

Acetyl bromide; In diethyl ether; at -78 - 0 ℃;
DOI:10.1021/ol0341492

Reference yield: 60.0%

: 75-36-5
acetyl chloride

: 25546-12-7
2,3,5-triiodobenzoic acid ethyl ester

: 524931-72-4
ethyl 2-acetyl-3,5-diiodobenzoate

Guidance literature:: 2,3,5-triiodobenzoic acid ethyl ester; With lithium dineopentylcuprate; In diethyl ether; at -78 ℃; for 0.333333h;

acetyl chloride; In diethyl ether; at -78 - 0 ℃;
DOI:10.1021/ol0341492

Reference yield:

: 88-82-4
2,3,5-triiodobenzoic acid

: 524931-72-4
ethyl 2-acetyl-3,5-diiodobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 95 percent / H₂SO₄ / Heating

2.1: lithium dineopentylcuprate / diethyl ether / 0.33 h / -78 °C

2.2: 70 percent / diethyl ether / -78 - 0 °C

With lithium dineopentylcuprate; sulfuric acid; In diethyl ether;
DOI:10.1021/ol0341492